XZ-150-151-A

Base Information

Chemical Name:XZ-150-151-A
CAS No.:1345992-96-2
Molecular Formula:C₃₀H₃₇N₅O₅Si
Molecular Weight:575.74
Hs Code.:

Synonyms:XZ-150-151-A

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Chemical Property of XZ-150-151-A

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Technology Process of XZ-150-151-A

There total 11 articles about XZ-150-151-A which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: XZ-150-147-A

: 1345992-96-2
XZ-150-151-A

Guidance literature:: With methanol; sodium methylate; 2-hydroxyethanethiol; for 5.5h; Reflux;
DOI:10.1016/j.tetlet.2011.09.074

Reference yield:

: 1-deoxy-1-methoxycarbonyl-5-O-tert-butyldiphenylsilyl-2,3-O-isopropyridene-β-D-ribofuranose

: 1345992-96-2
XZ-150-151-A

Guidance literature:: Multi-step reaction with 9 steps

1.1: diisobutylaluminium hydride / dichloromethane / 24 h / -78 - 20 °C

2.1: triethylamine / dichloromethane / 1.5 h / 0 - 20 °C

3.1: potassium tert-butylate / tetrahydrofuran / 2 h / 20 °C

4.1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / acetone / 4 h / 20 °C

5.1: sodium periodate; periodic acid / ethyl acetate / 3 h / 20 °C

6.1: sodium tetrahydroborate / ethyl acetate / 20 °C / Cooling with ice

7.1: dmap; triethylamine / dichloromethane / 4 h / Reflux

8.1: lithium hydride / dimethyl sulfoxide / 0.5 h / 90 °C / Inert atmosphere

8.2: 5 h / 90 °C / Inert atmosphere

9.1: methanol; sodium methylate; 2-hydroxyethanethiol / 5.5 h / Reflux

With methanol; dmap; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; potassium tert-butylate; water; sodium methylate; lithium hydride; diisobutylaluminium hydride; 4-methylmorpholine N-oxide; periodic acid; triethylamine; 2-hydroxyethanethiol; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; ethyl acetate; acetone;
DOI:10.1016/j.tetlet.2011.09.074

Reference yield:

: 1345992-82-6
C₂₆H₃₆O₅Si

: 1345992-96-2
XZ-150-151-A

Guidance literature:: Multi-step reaction with 8 steps

1.1: triethylamine / dichloromethane / 1.5 h / 0 - 20 °C

2.1: potassium tert-butylate / tetrahydrofuran / 2 h / 20 °C

3.1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / acetone / 4 h / 20 °C

4.1: sodium periodate; periodic acid / ethyl acetate / 3 h / 20 °C

5.1: sodium tetrahydroborate / ethyl acetate / 20 °C / Cooling with ice

6.1: dmap; triethylamine / dichloromethane / 4 h / Reflux

7.1: lithium hydride / dimethyl sulfoxide / 0.5 h / 90 °C / Inert atmosphere

7.2: 5 h / 90 °C / Inert atmosphere

8.1: methanol; sodium methylate; 2-hydroxyethanethiol / 5.5 h / Reflux

With methanol; dmap; sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; potassium tert-butylate; water; sodium methylate; lithium hydride; 4-methylmorpholine N-oxide; periodic acid; triethylamine; 2-hydroxyethanethiol; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; ethyl acetate; acetone;
DOI:10.1016/j.tetlet.2011.09.074