7-methoxy-2-naphthyl O-(2,3,4-tri-O-benzoyl-β-D-galactopyranosyl)-(1->4)-3-O-acetyl-2-O-dibenzyloxyphosphinyl-β-D-xylopyranoside

Base Information

Chemical Name:7-methoxy-2-naphthyl O-(2,3,4-tri-O-benzoyl-β-D-galactopyranosyl)-(1->4)-3-O-acetyl-2-O-dibenzyloxyphosphinyl-β-D-xylopyranoside
CAS No.:904684-09-9
Molecular Formula:C₅₉H₅₅O₁₈P
Molecular Weight:1083.05
Hs Code.:

Synonyms:7-methoxy-2-naphthyl O-(2,3,4-tri-O-benzoyl-β-D-galactopyranosyl)-(1->4)-3-O-acetyl-2-O-dibenzyloxyphosphinyl-β-D-xylopyranoside

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Chemical Property of 7-methoxy-2-naphthyl O-(2,3,4-tri-O-benzoyl-β-D-galactopyranosyl)-(1->4)-3-O-acetyl-2-O-dibenzyloxyphosphinyl-β-D-xylopyranoside

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Technology Process of 7-methoxy-2-naphthyl O-(2,3,4-tri-O-benzoyl-β-D-galactopyranosyl)-(1->4)-3-O-acetyl-2-O-dibenzyloxyphosphinyl-β-D-xylopyranoside

There total 4 articles about 7-methoxy-2-naphthyl O-(2,3,4-tri-O-benzoyl-β-D-galactopyranosyl)-(1->4)-3-O-acetyl-2-O-dibenzyloxyphosphinyl-β-D-xylopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 904684-08-8
7-methoxy-2-naphthyl O-(2,3,4-tri-O-benzoyl-6-O-levulinoyl-β-D-galactopyranosyl)-(1->4)-3-O-acetyl-2-O-dibenzyloxyphosphinyl-β-D-xylopyranoside

: 904684-09-9
7-methoxy-2-naphthyl O-(2,3,4-tri-O-benzoyl-β-D-galactopyranosyl)-(1->4)-3-O-acetyl-2-O-dibenzyloxyphosphinyl-β-D-xylopyranoside

Guidance literature:: With hydrazine hydrate; acetic acid; In pyridine; at 20 ℃; for 0.133333h;
DOI:10.1016/j.carres.2006.02.011

Reference yield:

: C₆₄H₆₁O₁₉P

: 904684-09-9
7-methoxy-2-naphthyl O-(2,3,4-tri-O-benzoyl-β-D-galactopyranosyl)-(1->4)-3-O-acetyl-2-O-dibenzyloxyphosphinyl-β-D-xylopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 724 mg / m-chloroperbenzoic acid / CH₂Cl₂ / 0.5 h / -10 °C

2: 93 percent / hydrazine hydrate; acetic acid / pyridine / 0.13 h / 20 °C

With hydrazine hydrate; acetic acid; 3-chloro-benzenecarboperoxoic acid; In pyridine; dichloromethane;
DOI:10.1016/j.carres.2006.02.011

Reference yield:

: 904684-06-6
7-methoxy-2-naphthyl O-(2,3,4-tri-O-benzoyl-6-O-levulinoyl-β-D-galactopyranosyl)-(1->4)-3-O-acetyl-β-D-xylopyranoside

: 904684-09-9
7-methoxy-2-naphthyl O-(2,3,4-tri-O-benzoyl-β-D-galactopyranosyl)-(1->4)-3-O-acetyl-2-O-dibenzyloxyphosphinyl-β-D-xylopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-tetrazole / CH₂Cl₂; acetonitrile / 1 h

2: 724 mg / m-chloroperbenzoic acid / CH₂Cl₂ / 0.5 h / -10 °C

3: 93 percent / hydrazine hydrate; acetic acid / pyridine / 0.13 h / 20 °C

With 1H-tetrazole; hydrazine hydrate; acetic acid; 3-chloro-benzenecarboperoxoic acid; In pyridine; dichloromethane; acetonitrile;
DOI:10.1016/j.carres.2006.02.011