phenoxycarbonyl 10ξ-cubebenyl sulfide

Base Information

Chemical Name:phenoxycarbonyl 10ξ-cubebenyl sulfide
CAS No.:137918-15-1
Molecular Formula:C₂₂H₂₈O₂S
Molecular Weight:356.529
Hs Code.:

Synonyms:phenoxycarbonyl 10ξ-cubebenyl sulfide

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Chemical Property of phenoxycarbonyl 10ξ-cubebenyl sulfide

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Technology Process of phenoxycarbonyl 10ξ-cubebenyl sulfide

There total 9 articles about phenoxycarbonyl 10ξ-cubebenyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 137917-99-8,138124-06-8
7(R*)-chloro-1-methyl-4(S*)-isopropyl-6(R*)-<1(R*)-(p-tolylsulfonyl)-4-(trimethylsilyl)-3-butynyl>bicyclo<3.1.1>heptan-6-ol

: 137918-15-1
phenoxycarbonyl 10ξ-cubebenyl sulfide

Guidance literature:: Multi-step reaction with 4 steps

1: 37 percent / Bu₃SnH, azobis(isobutyronitrile) (AIBN) / benzene / 48 h / Heating

2: 79 percent / p-toluenesulfinic acid, water / acetonitrile / 12 h / Heating

3: 67 percent / Na₂HPO₄, sodium amalgam / methanol; tetrahydrofuran / 1 h / -20 °C

4: 1.) KH, 2.) hexamethylphosphoramide (HMPA) / 1.) THF, 0.5 h, 2.) THF, 1 h

With N,N,N,N,N,N-hexamethylphosphoric triamide; disodium hydrogenphosphate; sodium amalgam; p-toluene sulfinic acid; 2,2'-azobis(isobutyronitrile); water; tri-n-butyl-tin hydride; potassium hydride; In tetrahydrofuran; methanol; acetonitrile; benzene;

Reference yield:

: 137918-00-4,138124-07-9
7(R*)-bromo-1-methyl-4(S*)-isopropyl-6(R*)-<1(R*)-(p-tolylsulfonyl)-4-(trimethylsilyl)-3-butynyl>bicyclo<3.1.1>heptan-6-ol

: 137918-15-1
phenoxycarbonyl 10ξ-cubebenyl sulfide

Guidance literature:: Multi-step reaction with 4 steps

1: 42 percent / Bu₃SnH, azobis(isobutyronitrile) (AIBN) / benzene / 3 h / Heating

2: 79 percent / p-toluenesulfinic acid, water / acetonitrile / 12 h / Heating

3: 67 percent / Na₂HPO₄, sodium amalgam / methanol; tetrahydrofuran / 1 h / -20 °C

4: 1.) KH, 2.) hexamethylphosphoramide (HMPA) / 1.) THF, 0.5 h, 2.) THF, 1 h

With N,N,N,N,N,N-hexamethylphosphoric triamide; disodium hydrogenphosphate; sodium amalgam; p-toluene sulfinic acid; 2,2'-azobis(isobutyronitrile); water; tri-n-butyl-tin hydride; potassium hydride; In tetrahydrofuran; methanol; acetonitrile; benzene;

Reference yield:

: 137918-11-7
7(R*)-bromo-1-methyl-4(S*)-isopropyl-6(R*)-<1(R*)-(p-tolylsulfonyl)-3-butynyl>bicyclo<3.1.1>heptan-6-ol

: 137918-15-1
phenoxycarbonyl 10ξ-cubebenyl sulfide

Guidance literature:: Multi-step reaction with 3 steps

1: Bu₃SnH, azobis(isobutyronitrile) (AIBN) / benzene / 3 h / Heating

2: 67 percent / Na₂HPO₄, sodium amalgam / methanol; tetrahydrofuran / 1 h / -20 °C

3: 1.) KH, 2.) hexamethylphosphoramide (HMPA) / 1.) THF, 0.5 h, 2.) THF, 1 h

With N,N,N,N,N,N-hexamethylphosphoric triamide; disodium hydrogenphosphate; sodium amalgam; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; potassium hydride; In tetrahydrofuran; methanol; benzene;