tert-butyl((3R,4R,E)-6-cyclohexyl-2,4-dimethylhexa-1,5-dien-3-yloxy)dimethylsilane

Base Information

Chemical Name:tert-butyl((3R,4R,E)-6-cyclohexyl-2,4-dimethylhexa-1,5-dien-3-yloxy)dimethylsilane
CAS No.:1017246-32-0
Molecular Formula:C₂₀H₃₈OSi
Molecular Weight:322.607
Hs Code.:

Synonyms:tert-butyl((3R,4R,E)-6-cyclohexyl-2,4-dimethylhexa-1,5-dien-3-yloxy)dimethylsilane

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Chemical Property of tert-butyl((3R,4R,E)-6-cyclohexyl-2,4-dimethylhexa-1,5-dien-3-yloxy)dimethylsilane

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Technology Process of tert-butyl((3R,4R,E)-6-cyclohexyl-2,4-dimethylhexa-1,5-dien-3-yloxy)dimethylsilane

There total 1 articles about tert-butyl((3R,4R,E)-6-cyclohexyl-2,4-dimethylhexa-1,5-dien-3-yloxy)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1017246-31-9
(3R,4R,E)-6-cyclohexyl-2,4-dimethylhexa-1,5-dien-3-ol

: 69739-34-0
t-butyldimethylsiyl triflate

: 1017246-32-0
tert-butyl((3R,4R,E)-6-cyclohexyl-2,4-dimethylhexa-1,5-dien-3-yloxy)dimethylsilane

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at -20 - 20 ℃; for 1.58333h; Inert atmosphere;
DOI:10.1021/ol702989g

Reference yield: 86.0%

: 1017246-32-0
tert-butyl((3R,4R,E)-6-cyclohexyl-2,4-dimethylhexa-1,5-dien-3-yloxy)dimethylsilane

: 1017246-33-1
(2S,3R,4R,E)-3-(tert-butyldimethylsilyloxy)-6-cyclohexyl-2,4-dimethylhex-5-en-1-ol

Guidance literature:: tert-butyl((3R,4R,E)-6-cyclohexyl-2,4-dimethylhexa-1,5-dien-3-yloxy)dimethylsilane; With 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; at -20 - 20 ℃; for 6.16667h; Inert atmosphere;

With sodium hydroxide; dihydrogen peroxide; In tetrahydrofuran; water; at 20 ℃; for 12h;
DOI:10.1021/ol702989g