Bicyclo[2.2.1]hept-5-ene-2-carboxylic acid, 2-amino-, (1R,2S,4R)-rel- (9CI)

Base Information

• Chemical Name: Bicyclo[2.2.1]hept-5-ene-2-carboxylic acid, 2-amino-, (1R,2S,4R)-rel- (9CI)
• CAS No.: 76637-59-7
• Molecular Formula: C₈H₁₁NO₂
• Molecular Weight: 153.181
• Mol file: 76637-59-7.mol

Synonyms:Bicyclo[2.2.1]hept-5-ene-2-carboxylicacid, 2-amino-, exo-

Chemical Property of Bicyclo[2.2.1]hept-5-ene-2-carboxylic acid, 2-amino-, (1R,2S,4R)-rel- (9CI)

Chemical Property:

• PSA: 63.32000
• LogP: 1.06480

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Bicyclo[2.2.1]hept-5-ene-2-carboxylic acid, 2-amino-, (1R,2S,4R)-rel- (9CI)

There total 5 articles about Bicyclo[2.2.1]hept-5-ene-2-carboxylic acid, 2-amino-, (1R,2S,4R)-rel- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 2-exo-amino<2.2.1>hept-5-ene-2-endo-carboxylate hydrochloride → 2-exo-amino<2.2.1>hept-5-ene-2-endo-carboxylic acid (76637-59-7)

Guidance literature:

With lithium hydroxide; In methanol; for 360h; Yield given; Ambient temperature;

DOI:10.1016/S0040-4020(01)87206-9

Reference yield:

methyl N--2-exo-amino<2.2.1>hept-5-ene-2-endo-carboxylate → 2-exo-amino<2.2.1>hept-5-ene-2-endo-carboxylic acid (76637-59-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / 0.5 N hydrochloric acid / tetrahydrofuran / 96 h / Ambient temperature

2: lithium hydroxide / methanol / 360 h / Ambient temperature

With hydrogenchloride; lithium hydroxide; In tetrahydrofuran; methanol;

DOI:10.1016/S0040-4020(01)87206-9

Reference yield:

methyl N--2-endo-amino<2.2.1>hept-5-ene-2-exo-carboxylate → 2-endo-amino<2.2.1>hept-5-ene-2-exo-carboxylic acid (76637-59-7)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / 0.5 N hydrochloric acid / tetrahydrofuran / 96 h / Ambient temperature

2: 1.) lithium hydroxide, 2.) Dowex-50H+ resin / 1.) methanol, room temp., 3 days

With hydrogenchloride; lithium hydroxide; Dowex-50H+ resin; In tetrahydrofuran;

DOI:10.1016/S0040-4020(01)87206-9

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 76637-59-7 Bicyclo[2.2.1]hept-5-ene-2-carboxylic acid, 2-amino-, (1R,2S,4R)-rel- (9CI)

Send

Send

Metric Ton KG G Pound L ML

Send

Send