C₃₂H₃₈O₆

Base Information

Chemical Name:C₃₂H₃₈O₆
CAS No.:1331832-24-6
Molecular Formula:C₃₂H₃₈O₆
Molecular Weight:518.65
Hs Code.:

C<sub>32</sub>H<sub>38</sub>O<sub>6</sub>

Synonyms:C₃₂H₃₈O₆

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₂H₃₈O₆

Chemical Property:

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Technology Process of C₃₂H₃₈O₆

There total 15 articles about C₃₂H₃₈O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1264756-66-2
C₃₂H₄₀O₆

: 1331832-24-6
C₃₂H₃₈O₆

Guidance literature:: With sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; potassium bromide; In dichloromethane; water; at 0 ℃; for 0.333333h;
DOI:10.1016/j.tet.2011.05.082

Reference yield:

: C₄₄H₅₂O₅Si

: 1331832-24-6
C₃₂H₃₈O₆

Guidance literature:: Multi-step reaction with 10 steps

1.1: water; potassium hydroxide / tetrahydrofuran; methanol

2.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 - 20 °C

2.2: 20 °C

3.1: diisobutylaluminium hydride / dichloromethane / -78 °C

4.1: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -40 °C / Molecular sieve

5.1: sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; potassium bromide / dichloromethane; water / 0 °C

6.1: sodium hexamethyldisilazane / tetrahydrofuran / 0 °C

7.1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 20 °C

8.1: potassium tert-butylate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 20 °C

9.1: bis-(1,2-dimethylpropyl)borane / tetrahydrofuran / 0 - 20 °C

9.2: 20 °C

10.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 20 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium hypochlorite; oxalyl dichloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; diethyl (2R,3R)-tartrate; potassium tert-butylate; water; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; bis-(1,2-dimethylpropyl)borane; tetra-(n-butyl)ammonium iodide; diisobutylaluminium hydride; sodium hydrogencarbonate; dimethyl sulfoxide; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; potassium bromide; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; 2.1: Swern oxidation / 2.2: Wittig reaction / 4.1: Sharpless asymmetric epoxidation / 6.1: Wittig reaction;
DOI:10.1016/j.tetlet.2010.11.127

Reference yield:

: 1264756-61-7
C₂₈H₃₄O₅

: 1331832-24-6
C₃₂H₃₈O₆

Guidance literature:: Multi-step reaction with 9 steps

1.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 - 20 °C

1.2: 20 °C

2.1: diisobutylaluminium hydride / dichloromethane / -78 °C

3.1: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / -40 °C / Molecular sieve

4.1: sodium hypochlorite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate; potassium bromide / dichloromethane; water / 0 °C

5.1: sodium hexamethyldisilazane / tetrahydrofuran / 0 °C

6.1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 20 °C

7.1: potassium tert-butylate; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 20 °C

8.1: bis-(1,2-dimethylpropyl)borane / tetrahydrofuran / 0 - 20 °C

8.2: 20 °C

9.1: sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine / dichloromethane / 20 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium hypochlorite; oxalyl dichloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; diethyl (2R,3R)-tartrate; potassium tert-butylate; water; sodium hexamethyldisilazane; sulfur trioxide pyridine complex; bis-(1,2-dimethylpropyl)borane; tetra-(n-butyl)ammonium iodide; diisobutylaluminium hydride; sodium hydrogencarbonate; dimethyl sulfoxide; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; potassium bromide; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; 1.1: Swern oxidation / 1.2: Wittig reaction / 3.1: Sharpless asymmetric epoxidation / 5.1: Wittig reaction;
DOI:10.1016/j.tetlet.2010.11.127