C₂₇H₃₀BrN₂O⁽¹⁺⁾*Cl^(1-)

Base Information

• Chemical Name: C₂₇H₃₀BrN₂O⁽¹⁺⁾*Cl^(1-)
• CAS No.: 1403227-05-3
• Molecular Formula: C₂₇H₃₀BrN₂O*Cl
• Molecular Weight: 513.905
• Mol file: 1403227-05-3.mol

Synonyms:C₂₇H₃₀BrN₂O⁽¹⁺⁾*Cl^(1-)

Chemical Property of C₂₇H₃₀BrN₂O⁽¹⁺⁾*Cl^(1-)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₂₇H₃₀BrN₂O⁽¹⁺⁾*Cl^(1-)

There total 1 articles about C₂₇H₃₀BrN₂O⁽¹⁺⁾*Cl^(1-) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

4-bromo-benzaldehyde (1122-91-4) + 3-diethylaminophenol (91-68-9) → C27H30BrN2O(1+)*Cl(1-) (1403227-05-3)

Guidance literature:

4-bromo-benzaldehyde; 3-diethylaminophenol; With toluene-4-sulfonic acid; acetic acid; at 70 ℃; for 7h;

With sodium hydroxide; at 20 ℃;

With chloranil; In dichloromethane; for 2h;

DOI:10.1002/ejic.201100777

Reference yield:

C27H30BrN2O(1+)*Cl(1-) (1403227-05-3) + trimethylsilylacetylene (1066-54-2) → C32H39N2OSi(1+)*Cl(1-)

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine; In tetrahydrofuran; at 70 ℃; for 7h; Inert atmosphere;

DOI:10.1002/ejic.201100777

upstream raw materials:

4-bromo-benzaldehyde

3-diethylaminophenol