1-(4-((tert-butyldimethylsilyloxy)methyl)phenyl)-2,2,3,3,4,4,4-heptafluorobutan-1-one

Base Information

Chemical Name:1-(4-((tert-butyldimethylsilyloxy)methyl)phenyl)-2,2,3,3,4,4,4-heptafluorobutan-1-one
CAS No.:1191250-87-9
Molecular Formula:C₁₇H₂₁F₇O₂Si
Molecular Weight:418.427
Hs Code.:

Synonyms:1-(4-((tert-butyldimethylsilyloxy)methyl)phenyl)-2,2,3,3,4,4,4-heptafluorobutan-1-one

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Chemical Property of 1-(4-((tert-butyldimethylsilyloxy)methyl)phenyl)-2,2,3,3,4,4,4-heptafluorobutan-1-one

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Technology Process of 1-(4-((tert-butyldimethylsilyloxy)methyl)phenyl)-2,2,3,3,4,4,4-heptafluorobutan-1-one

There total 1 articles about 1-(4-((tert-butyldimethylsilyloxy)methyl)phenyl)-2,2,3,3,4,4,4-heptafluorobutan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 754-34-7
1,1,1,2,2,3,3-heptafluoro-3-iodo-propane

: 139706-48-2
4-(tert-butyldimethylsilyloxymethyl)benzoic acid methyl ester

: 1191250-87-9
1-(4-((tert-butyldimethylsilyloxy)methyl)phenyl)-2,2,3,3,4,4,4-heptafluorobutan-1-one

Guidance literature:: 1,1,1,2,2,3,3-heptafluoro-3-iodo-propane; With isopropylmagnesium chloride; In tetrahydrofuran; diethyl ether; at -78 ℃; for 1h; Inert atmosphere;

4-(tert-butyldimethylsilyloxymethyl)benzoic acid methyl ester; In tetrahydrofuran; diethyl ether; at -78 - 0 ℃;
DOI:10.1021/ol901955y

Reference yield: 50.0%

: 1191250-87-9
1-(4-((tert-butyldimethylsilyloxy)methyl)phenyl)-2,2,3,3,4,4,4-heptafluorobutan-1-one

: 98-59-9
p-toluenesulfonyl chloride

: 1191250-89-1
1-(4-((tert-butyldimethylsilyloxy)methyl)phenyl)-2,2,3,3,4,4,4-heptafluorobutan-1-one o-tosyl oxime

Guidance literature:: 1-(4-((tert-butyldimethylsilyloxy)methyl)phenyl)-2,2,3,3,4,4,4-heptafluorobutan-1-one; With pyridine; hydroxylamine hydrochloride; In ethanol; at 20 - 85 ℃;

p-toluenesulfonyl chloride; With pyridine; In dichloromethane; at 85 ℃; for 16h;
DOI:10.1021/ol901955y