HCCC₆H₄C₂CH₂OH

Base Information

Chemical Name:HCCC₆H₄C₂CH₂OH
CAS No.:539021-47-1
Molecular Formula:C₁₁H₈O
Molecular Weight:156.184
Hs Code.:

HCCC<sub>6</sub>H<sub>4</sub>C<sub>2</sub>CH<sub>2</sub>OH

Synonyms:HCCC₆H₄C₂CH₂OH

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Chemical Property of HCCC₆H₄C₂CH₂OH

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Technology Process of HCCC₆H₄C₂CH₂OH

There total 4 articles about HCCC₆H₄C₂CH₂OH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 80151-10-6
4-(3-hydroxy-1-propyn-1-yl)-benzaldehyde

: 4202-14-6
dimethyl (2-oxopropyl)phosphonate

: 539021-47-1
HCCC₆H₄C₂CH₂OH

Guidance literature:: dimethyl (2-oxopropyl)phosphonate; With 4-toluenesulfonyl azide; potassium carbonate; In acetonitrile; at 25 ℃; for 2h; Inert atmosphere;

4-(3-hydroxy-1-propyn-1-yl)-benzaldehyde; In methanol; acetonitrile; at 25 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ja1071916

Reference yield:

: 1122-91-4
4-bromo-benzaldehyde

: 539021-47-1
HCCC₆H₄C₂CH₂OH

Guidance literature:: Multi-step reaction with 2 steps

1.1: copper(l) iodide; sodium tetrachloropalladate(II); N,N,N,N,-tetramethylethylenediamine; di‐tert‐butyl‐(1‐phenylindol‐2‐yl)phosphane / 12 h / 80 °C / Inert atmosphere

2.1: 4-toluenesulfonyl azide; potassium carbonate / acetonitrile / 2 h / 25 °C / Inert atmosphere

2.2: 12 h / 25 °C / Inert atmosphere

With copper(l) iodide; 4-toluenesulfonyl azide; sodium tetrachloropalladate(II); N,N,N,N,-tetramethylethylenediamine; potassium carbonate; di‐tert‐butyl‐(1‐phenylindol‐2‐yl)phosphane; In acetonitrile; 2.1: Ohira-Bestmann reaction / 2.2: Ohira-Bestmann reaction;
DOI:10.1021/ja1071916