1-Bicyclo<2.2.2>octyl Cyclohexyl Ketone

Base Information

Chemical Name:1-Bicyclo<2.2.2>octyl Cyclohexyl Ketone
CAS No.:74467-38-2
Molecular Formula:C₁₅H₂₄O
Molecular Weight:220.355
Hs Code.:

Synonyms:1-Bicyclo<2.2.2>octyl Cyclohexyl Ketone

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Chemical Property of 1-Bicyclo<2.2.2>octyl Cyclohexyl Ketone

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Technology Process of 1-Bicyclo<2.2.2>octyl Cyclohexyl Ketone

There total 5 articles about 1-Bicyclo<2.2.2>octyl Cyclohexyl Ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 931-98-6
1-Iodobicyclo<2.2.2>octane

: 2719-27-9
cyclohexanylcarbonyl chloride

: 74467-38-2
1-Bicyclo<2.2.2>octyl Cyclohexyl Ketone

Guidance literature:: With tert.-butyl lithium; In diethyl ether; pentane; at -78 ℃;
DOI:10.1021/jo01308a001

Reference yield:

: 20534-58-1
bicyclo[2.2.2]octan-1-ol

: 74467-38-2
1-Bicyclo<2.2.2>octyl Cyclohexyl Ketone

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / Hydriodic acid / acetic acid / 1 h / Heating

2: 92 percent / tert-butyllithium / diethyl ether; pentane / -78 °C

With hydrogen iodide; tert.-butyl lithium; In diethyl ether; acetic acid; pentane;
DOI:10.1021/jo01308a001

Reference yield:

: 1123-39-3
1,4-Dichloro-bicyclo<2.2.2>octane

: 74467-38-2
1-Bicyclo<2.2.2>octyl Cyclohexyl Ketone

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / C₂H₅I, AlBr₃

2: 1.) Silver acetate; 2.) Potassium hydroxide / 1.) Glacial acetic acid, Reflux for 1 h; 2.) Ethanol, Reflux 2 h

3: 62.4 percent / tert-butyllithium / diethyl ether; pentane; methanol

4: 89 percent / Hydriodic acid / acetic acid / 1 h / Heating

5: 92 percent / tert-butyllithium / diethyl ether; pentane / -78 °C

With potassium hydroxide; aluminum tri-bromide; hydrogen iodide; tert.-butyl lithium; silver(I) acetate; ethyl iodide; In methanol; diethyl ether; acetic acid; pentane;
DOI:10.1021/jo01308a001