(E)-3-Phenyl-acrylic acid (2S,3S,5R,6R)-5,6-dimethoxy-5,6-dimethyl-3-[(E)-(3-phenyl-acryloyl)oxymethyl]-[1,4]dioxan-2-ylmethyl ester

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Chemical Name:(E)-3-Phenyl-acrylic acid (2S,3S,5R,6R)-5,6-dimethoxy-5,6-dimethyl-3-[(E)-(3-phenyl-acryloyl)oxymethyl]-[1,4]dioxan-2-ylmethyl ester
CAS No.:181586-75-4
Molecular Formula:C₂₈H₃₂O₈
Molecular Weight:496.557
Hs Code.:

Synonyms:(E)-3-Phenyl-acrylic acid (2S,3S,5R,6R)-5,6-dimethoxy-5,6-dimethyl-3-[(E)-(3-phenyl-acryloyl)oxymethyl]-[1,4]dioxan-2-ylmethyl ester

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Chemical Property of (E)-3-Phenyl-acrylic acid (2S,3S,5R,6R)-5,6-dimethoxy-5,6-dimethyl-3-[(E)-(3-phenyl-acryloyl)oxymethyl]-[1,4]dioxan-2-ylmethyl ester

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Technology Process of (E)-3-Phenyl-acrylic acid (2S,3S,5R,6R)-5,6-dimethoxy-5,6-dimethyl-3-[(E)-(3-phenyl-acryloyl)oxymethyl]-[1,4]dioxan-2-ylmethyl ester

There total 5 articles about (E)-3-Phenyl-acrylic acid (2S,3S,5R,6R)-5,6-dimethoxy-5,6-dimethyl-3-[(E)-(3-phenyl-acryloyl)oxymethyl]-[1,4]dioxan-2-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 102-92-1,17082-09-6
Cinnamoyl chloride

: 173371-55-6
(2S,3S,5R,6R)-2,3-bis(hydroxymethyl)-5,6-dimethoxy-5,6-dimethyl<1,4>dioxane

: 181586-75-4
(E)-3-Phenyl-acrylic acid (2S,3S,5R,6R)-5,6-dimethoxy-5,6-dimethyl-3-[(E)-(3-phenyl-acryloyl)oxymethyl]-[1,4]dioxan-2-ylmethyl ester

Guidance literature:: With dmap; In pyridine; dichloromethane; for 20h; Ambient temperature;
DOI:10.1021/jo960556y

Reference yield:

: 21983-72-2
3,3-dimethoxy-butan-2-one

: 181586-75-4
(E)-3-Phenyl-acrylic acid (2S,3S,5R,6R)-5,6-dimethoxy-5,6-dimethyl-3-[(E)-(3-phenyl-acryloyl)oxymethyl]-[1,4]dioxan-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: p-toluenesulfonic acid / 4 h / 70 °C / 70 Torr

2: 95 percent / LiAlH₄ / tetrahydrofuran / 3 h / Heating

3: 96 percent / DMAP / CH₂Cl₂; pyridine / 20 h / Ambient temperature

With dmap; lithium aluminium tetrahydride; toluene-4-sulfonic acid; In tetrahydrofuran; pyridine; dichloromethane;
DOI:10.1021/jo960556y

Reference yield:

: 181586-79-8
(2S,3S,5R,6R)-2,3-bis([(indene-2-carbonyl)oxy]methyl)-5,6-dimethoxy-5,6-dimethyl[1,4]dioxane

: 181586-75-4
(E)-3-Phenyl-acrylic acid (2S,3S,5R,6R)-5,6-dimethoxy-5,6-dimethyl-3-[(E)-(3-phenyl-acryloyl)oxymethyl]-[1,4]dioxan-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 48 percent / toluene / 36 h / -70 °C / Irradiation

2: 97 percent / LiAlH₄ / tetrahydrofuran / Ambient temperature

3: 96 percent / DMAP / CH₂Cl₂; pyridine / 20 h / Ambient temperature

With dmap; lithium aluminium tetrahydride; In tetrahydrofuran; pyridine; dichloromethane; toluene;
DOI:10.1021/jo960556y