1-O-allyl-2,3,4,5-tetra-O-benzyl-6-O-(2-O-benzoyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-D-myo-inositol

Base Information

Chemical Name:1-O-allyl-2,3,4,5-tetra-O-benzyl-6-O-(2-O-benzoyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-D-myo-inositol
CAS No.:312538-73-1
Molecular Formula:C₇₁H₇₂O₁₂
Molecular Weight:1117.35
Hs Code.:

Synonyms:1-O-allyl-2,3,4,5-tetra-O-benzyl-6-O-(2-O-benzoyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-D-myo-inositol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-O-allyl-2,3,4,5-tetra-O-benzyl-6-O-(2-O-benzoyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-D-myo-inositol

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Technology Process of 1-O-allyl-2,3,4,5-tetra-O-benzyl-6-O-(2-O-benzoyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-D-myo-inositol

There total 1 articles about 1-O-allyl-2,3,4,5-tetra-O-benzyl-6-O-(2-O-benzoyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-D-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 132437-54-8
1-O-allyl-2,3,4,5-tetra-O-benzyl-D-myo-inositol

: 125392-62-3
3,4,6-tri-O-benzyl-β-D-mannopyranose 1,2-(pent-4-enyl orthobenzoate)

: 312538-73-1
1-O-allyl-2,3,4,5-tetra-O-benzyl-6-O-(2-O-benzoyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-D-myo-inositol

Guidance literature:: With N-iodo-succinimide; t-butyldimethylsiyl triflate; at 20 ℃; for 0.333333h;
DOI:10.1016/S0040-4039(00)01329-0

Reference yield: 95.0%

: 312538-73-1
1-O-allyl-2,3,4,5-tetra-O-benzyl-6-O-(2-O-benzoyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-D-myo-inositol

: 312631-42-8
1-O-allyl-2,3,4,5-tetra-O-benzyl-6-O-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-D-myo-inositol

Guidance literature:: With methanol; sodium methylate; In dichloromethane; for 14h;
DOI:10.1560/KDP7-D0BA-BN04-3H3A

Reference yield:

: 312538-73-1
1-O-allyl-2,3,4,5-tetra-O-benzyl-6-O-(2-O-benzoyl-3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-D-myo-inositol

: (2R,4S,5R,6R)-2-((1S,2R,3S,4S,5R,6S)-2-Allyloxy-3,4,5,6-tetrakis-benzyloxy-cyclohexyloxy)-4,5-bis-benzyloxy-6-benzyloxymethyl-dihydro-pyran-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / NaOMe; MeOH / CH₂Cl₂ / 14 h

2: Ac₂O; DMSO / 16 h

With methanol; sodium methylate; acetic anhydride; dimethyl sulfoxide; In dichloromethane;
DOI:10.1560/KDP7-D0BA-BN04-3H3A