Acetic acid 1'-acetoxy-4,4'-bis-(3-acetylamino-phenyl)-6,8,6',8'-tetramethoxy-[2,2']binaphthalenyl-1-yl ester

Base Information

Chemical Name:Acetic acid 1'-acetoxy-4,4'-bis-(3-acetylamino-phenyl)-6,8,6',8'-tetramethoxy-[2,2']binaphthalenyl-1-yl ester
CAS No.:198494-13-2
Molecular Formula:C₄₄H₄₀N₂O₁₀
Molecular Weight:756.809
Hs Code.:

Synonyms:Acetic acid 1'-acetoxy-4,4'-bis-(3-acetylamino-phenyl)-6,8,6',8'-tetramethoxy-[2,2']binaphthalenyl-1-yl ester

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Chemical Property of Acetic acid 1'-acetoxy-4,4'-bis-(3-acetylamino-phenyl)-6,8,6',8'-tetramethoxy-[2,2']binaphthalenyl-1-yl ester

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Technology Process of Acetic acid 1'-acetoxy-4,4'-bis-(3-acetylamino-phenyl)-6,8,6',8'-tetramethoxy-[2,2']binaphthalenyl-1-yl ester

There total 8 articles about Acetic acid 1'-acetoxy-4,4'-bis-(3-acetylamino-phenyl)-6,8,6',8'-tetramethoxy-[2,2']binaphthalenyl-1-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78887-39-5
3-Acetamidophenylboronic acid

: 198494-28-9
Acetic acid 1'-acetoxy-6,8,6',8'-tetramethoxy-4,4'-bis-trifluoromethanesulfonyloxy-[2,2']binaphthalenyl-1-yl ester

: 198494-13-2
Acetic acid 1'-acetoxy-4,4'-bis-(3-acetylamino-phenyl)-6,8,6',8'-tetramethoxy-[2,2']binaphthalenyl-1-yl ester

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; barium dihydroxide; In N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(97)10057-9

Reference yield:

: 36440-19-4
5,7-dimethoxy-1,4-naphthoquinone

: 198494-13-2
Acetic acid 1'-acetoxy-4,4'-bis-(3-acetylamino-phenyl)-6,8,6',8'-tetramethoxy-[2,2']binaphthalenyl-1-yl ester

Guidance literature:: Multi-step reaction with 8 steps

1: aq. Na₂S₂O₄ / ethyl acetate

2: HCl gas

3: Ag₂O, Et₃N / CH₂Cl₂

4: conc. HNO₃ / 0.03 h

5: Zn, NaOAc, DMAP / CH₂Cl₂

6: DBU

8: PdCl₂(dppf), Ba(OH)2 / dimethylformamide

With hydrogenchloride; dmap; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; barium dihydroxide; sodium dithionite; nitric acid; sodium acetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; silver(l) oxide; zinc; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(97)10057-9

Reference yield:

: 91963-81-4
1,4-Dihydroxy-5,7-dimethoxy-naphthalin

: 198494-13-2
Acetic acid 1'-acetoxy-4,4'-bis-(3-acetylamino-phenyl)-6,8,6',8'-tetramethoxy-[2,2']binaphthalenyl-1-yl ester

Guidance literature:: Multi-step reaction with 7 steps

1: HCl gas

2: Ag₂O, Et₃N / CH₂Cl₂

3: conc. HNO₃ / 0.03 h

4: Zn, NaOAc, DMAP / CH₂Cl₂

5: DBU

7: PdCl₂(dppf), Ba(OH)2 / dimethylformamide

With hydrogenchloride; dmap; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; barium dihydroxide; nitric acid; sodium acetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; silver(l) oxide; zinc; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(97)10057-9