2-(4-(3,5-dimethoxyphenyl)cyclohexylidene)-1-(4-iodobenzyl)-1-phenylhydrazine

Base Information

Chemical Name:2-(4-(3,5-dimethoxyphenyl)cyclohexylidene)-1-(4-iodobenzyl)-1-phenylhydrazine
CAS No.:1344674-53-8
Molecular Formula:C₂₇H₂₉IN₂O₂
Molecular Weight:540.444
Hs Code.:

Synonyms:2-(4-(3,5-dimethoxyphenyl)cyclohexylidene)-1-(4-iodobenzyl)-1-phenylhydrazine

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Chemical Property of 2-(4-(3,5-dimethoxyphenyl)cyclohexylidene)-1-(4-iodobenzyl)-1-phenylhydrazine

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Technology Process of 2-(4-(3,5-dimethoxyphenyl)cyclohexylidene)-1-(4-iodobenzyl)-1-phenylhydrazine

There total 4 articles about 2-(4-(3,5-dimethoxyphenyl)cyclohexylidene)-1-(4-iodobenzyl)-1-phenylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1297474-29-3
4-(3,5-dimethoxyphenyl)cyclohexan-1-one

: 1344674-97-0
1-(4-iodobenzyl)-1-phenylhydrazine

: 1344674-53-8
2-(4-(3,5-dimethoxyphenyl)cyclohexylidene)-1-(4-iodobenzyl)-1-phenylhydrazine

Guidance literature:: With acetic acid; In ethanol; at 60 ℃; for 3h;
DOI:10.1021/ja2092163

Reference yield:

: 8-(3,5-dimethoxyphenyl)-1,4-dioxaspiro[4.5]dec-7-ene

: 1344674-53-8
2-(4-(3,5-dimethoxyphenyl)cyclohexylidene)-1-(4-iodobenzyl)-1-phenylhydrazine

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / methanol; ethyl acetate / 20 °C

2: hydrogenchloride / tetrahydrofuran; water / Reflux

3: acetic acid / ethanol / 3 h / 60 °C

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; acetic acid; In tetrahydrofuran; methanol; ethanol; water; ethyl acetate;
DOI:10.1021/ja2092163

Reference yield:

: 1297474-23-7
C₁₆H₂₂O₅

: 1344674-53-8
2-(4-(3,5-dimethoxyphenyl)cyclohexylidene)-1-(4-iodobenzyl)-1-phenylhydrazine

Guidance literature:: Multi-step reaction with 4 steps

1: toluene-4-sulfonic acid / toluene / 100 °C

2: palladium 10% on activated carbon; hydrogen / methanol; ethyl acetate / 20 °C

3: hydrogenchloride / tetrahydrofuran; water / Reflux

4: acetic acid / ethanol / 3 h / 60 °C

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; toluene-4-sulfonic acid; acetic acid; In tetrahydrofuran; methanol; ethanol; water; ethyl acetate; toluene;
DOI:10.1021/ja2092163