<2S-(2a(αS,βR),3aα,4β,7β,7aα)>-α-methyl-β-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy>benzolethanamin

Base Information

Chemical Name:<2S-(2a(αS*,βR*),3aα,4β,7β,7aα)>-α-methyl-β-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy>benzolethanamin
CAS No.:133735-62-3
Molecular Formula:C₂₁H₃₁NO₂
Molecular Weight:329.483
Hs Code.:

Synonyms:<2S-(2a(αS*,βR*),3aα,4β,7β,7aα)>-α-methyl-β-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy>benzolethanamin

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Chemical Property of <2S-(2a(αS*,βR*),3aα,4β,7β,7aα)>-α-methyl-β-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy>benzolethanamin

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Technology Process of <2S-(2a(αS*,βR*),3aα,4β,7β,7aα)>-α-methyl-β-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy>benzolethanamin

There total 4 articles about <2S-(2a(αS*,βR*),3aα,4β,7β,7aα)>-α-methyl-β-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy>benzolethanamin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 532-28-5,613-88-7
(RS)-mandelonitrile

: 133735-62-3,133812-93-8,135028-69-2,135028-70-5,135028-71-6
(R)-1-Methyl-2-phenyl-2-((1R,2R,4S,6R,7R)-1,10,10-trimethyl-3-oxa-tricyclo[5.2.1.0^2,6]dec-4-yloxy)-ethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 25.2 percent / p-TsOH / CH₂Cl₂ / 2 h / Ambient temperature

2: 2) LiAlH₄ / 1) ether, 2 h, room temp., 2) 15 h, -50 deg C up to 10 deg C

With lithium aluminium tetrahydride; toluene-4-sulfonic acid; In dichloromethane;
DOI:10.1007/BF00810829

Reference yield:

: 532-28-5,613-88-7
(RS)-mandelonitrile

: 133735-62-3
<2S-(2a(αS*,βR*),3aα,4β,7β,7aα)>-α-methyl-β-<(octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-yl)oxy>benzolethanamin

Guidance literature:: Multi-step reaction with 2 steps

1: 35.7 percent / p-TsOH / CH₂Cl₂ / 2 h / Ambient temperature

2: 2) LiAlH₄ / 1) ether, 2 h, room temp., 2) 15 h, -50 deg C up to 10 deg C

With lithium aluminium tetrahydride; toluene-4-sulfonic acid; In dichloromethane;
DOI:10.1007/BF00810829

Reference yield:

: 108031-76-1
<2R-(2α,3aα,4β,7β,7aα)>-Octahydro-7,8,8-trimethyl-4,7-methanobenzofuran-2-ol

: 133735-62-3,133812-93-8,135028-69-2,135028-70-5,135028-71-6
(R)-1-Methyl-2-phenyl-2-((1R,2R,4S,6R,7R)-1,10,10-trimethyl-3-oxa-tricyclo[5.2.1.0^2,6]dec-4-yloxy)-ethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 25.2 percent / p-TsOH / CH₂Cl₂ / 2 h / Ambient temperature

2: 2) LiAlH₄ / 1) ether, 2 h, room temp., 2) 15 h, -50 deg C up to 10 deg C

With lithium aluminium tetrahydride; toluene-4-sulfonic acid; In dichloromethane;
DOI:10.1007/BF00810829