[(3-hydroxy-4-chlorophenyl)-2-methoxy(D₃)-methylene]-5-methoxy(D₃)adamantane

Base Information

• Chemical Name: [(3-hydroxy-4-chlorophenyl)-2-methoxy(D₃)-methylene]-5-methoxy(D₃)adamantane
• CAS No.: 552848-20-1
• Molecular Formula: C₁₉H₂₃ClO₃
• Molecular Weight: 340.795

Synonyms:[(3-hydroxy-4-chlorophenyl)-2-methoxy(D₃)-methylene]-5-methoxy(D₃)adamantane

Chemical Property of [(3-hydroxy-4-chlorophenyl)-2-methoxy(D₃)-methylene]-5-methoxy(D₃)adamantane

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Technology Process of [(3-hydroxy-4-chlorophenyl)-2-methoxy(D₃)-methylene]-5-methoxy(D₃)adamantane

There total 1 articles about [(3-hydroxy-4-chlorophenyl)-2-methoxy(D₃)-methylene]-5-methoxy(D₃)adamantane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[(3-t-butyldimethylsilyloxy-4-chlorophenyl)-2-methoxy(D3)-methylene]-5-methoxy(D3)adamantane (552848-19-8) → [(3-hydroxy-4-chlorophenyl)-2-methoxy(D3)-methylene]-5-methoxy(D3)adamantane (552848-20-1)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 1.66667h;

Reference yield:

sodium hydroxide (1310-73-2) + [(3-hydroxy-4-chlorophenyl)-2-methoxy(D3)-methylene]-5-methoxy(D3)adamantane (552848-20-1) → [(3-phosphoryloxy-4-chlorophenyl)-2-methoxy(D3)-methylene]-5-methoxy(D3)adamantane disodium salt

Guidance literature:

[(3-hydroxy-4-chlorophenyl)-2-methoxy(D₃)-methylene]-5-methoxy(D₃)adamantane; With pyridine; trichlorophosphate; In tetrahydrofuran; at 0 - 20 ℃; for 3.83333h;

With pyridine; 3-Hydroxypropionitrile; In tetrahydrofuran; at 20 ℃; for 20.5833h;

sodium hydroxide; With water; In acetonitrile; for 2.33333h;

upstream raw materials:

[(3-t-butyldimethylsilyloxy-4-chlorophenyl)-2-methoxy(D₃)-methylene]-5-methoxy(D₃)adamantane

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