C₃₅H₄₀ClN₃O₄S

Base Information

Chemical Name:C₃₅H₄₀ClN₃O₄S
CAS No.:1382034-64-1
Molecular Formula:C₃₅H₄₀ClN₃O₄S
Molecular Weight:634.239
Hs Code.:

C<sub>35</sub>H<sub>40</sub>ClN<sub>3</sub>O<sub>4</sub>S

Synonyms:C₃₅H₄₀ClN₃O₄S

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Chemical Property of C₃₅H₄₀ClN₃O₄S

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Technology Process of C₃₅H₄₀ClN₃O₄S

There total 7 articles about C₃₅H₄₀ClN₃O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 916204-05-2
4-(4-((4'-chlorobiphenyl-2-yl)methyl)piperazin-1-yl)benzoic acid

: 1382034-60-7
(3-hydroxyadamantan-1-yl)methanesulfonamide

: 1382034-64-1
C₃₅H₄₀ClN₃O₄S

Guidance literature:: 4-(4-((4'-chlorobiphenyl-2-yl)methyl)piperazin-1-yl)benzoic acid; With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 1h; Inert atmosphere;

(3-hydroxyadamantan-1-yl)methanesulfonamide; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1021/ml300095a

Reference yield:

: 1382034-59-4
(3-bromoadamantan-1-yl)methanesulfonamide

: 1382034-64-1
C₃₅H₄₀ClN₃O₄S

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium dihydrogenphosphate / water / 0.17 h / 180 °C / Microwave irradiation; Inert atmosphere

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane; N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

With sodium dihydrogenphosphate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ml300095a

Reference yield:

: C₁₁H₁₆BrI

: 1382034-64-1
C₃₅H₄₀ClN₃O₄S

Guidance literature:: Multi-step reaction with 5 steps

1.1: tetrahydrofuran / 60 °C / Inert atmosphere

2.1: sulfuryl dichloride; acetic anhydride / 1,2-dichloro-ethane / 0.5 h / -10 °C / Inert atmosphere

2.2: Inert atmosphere; Cooling with ice

3.1: potassium permanganate / water; acetone / 2 h / 50 °C / Inert atmosphere

4.1: sodium dihydrogenphosphate / water / 0.17 h / 180 °C / Microwave irradiation; Inert atmosphere

5.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane; N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

5.2: 20 °C / Inert atmosphere

With potassium permanganate; sodium dihydrogenphosphate; sulfuryl dichloride; acetic anhydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone;
DOI:10.1021/ml300095a