5-benzyl-5H-pyrido[3,2-b]indole

Base Information

Chemical Name:5-benzyl-5H-pyrido[3,2-b]indole
CAS No.:1346545-68-3
Molecular Formula:C₁₈H₁₄N₂
Molecular Weight:258.323
Hs Code.:

Synonyms:5-benzyl-5H-pyrido[3,2-b]indole

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Chemical Property of 5-benzyl-5H-pyrido[3,2-b]indole

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Technology Process of 5-benzyl-5H-pyrido[3,2-b]indole

There total 7 articles about 5-benzyl-5H-pyrido[3,2-b]indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1312012-32-0
3-bromo-2-(2-bromophenyl)pyridine

: 100-46-9
benzylamine

: 1346545-68-3
5-benzyl-5H-pyrido[3,2-b]indole

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; bis[2-(diphenylphosphino)phenyl] ether; sodium t-butanolate; In toluene; at 100 ℃; for 7h; Sealed tube; Inert atmosphere;
DOI:10.1039/c4ob02226b

Reference yield: 65.0%

: 1360168-61-1
benzo[4,5]pyrido[3,2-b]iodol-5-ium trifluoromethanesulfonate

: 100-46-9
benzylamine

: 1346545-68-3
5-benzyl-5H-pyrido[3,2-b]indole

Guidance literature:: benzo[4,5]pyrido[3,2-b]iodol-5-ium trifluoromethanesulfonate; With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In toluene; at 20 ℃; for 0.0833333h; Inert atmosphere;

benzylamine; In toluene; at 100 ℃; for 16h; Inert atmosphere;
DOI:10.1055/s-0031-1289652

Reference yield:

: 244205-40-1
(2-bromophenyl)boronic acid

: 1346545-68-3
5-benzyl-5H-pyrido[3,2-b]indole

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydroxide / tetrahydrofuran; water / 4 h / 70 °C / Schlenk technique; Inert atmosphere

2: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium t-butanolate; bis[2-(diphenylphosphino)phenyl] ether / toluene / 7 h / 100 °C / Sealed tube; Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tetrakis(triphenylphosphine) palladium⁽⁰⁾; bis[2-(diphenylphosphino)phenyl] ether; sodium hydroxide; sodium t-butanolate; In tetrahydrofuran; water; toluene; 1: |Suzuki-Miyaura Coupling;
DOI:10.1039/c4ob02226b