3-[bis(diisopropylamino)phosphino]-1-methyl-2-phenyl-3H-imidazol-3-ium triflate

Base Information

• Chemical Name: 3-[bis(diisopropylamino)phosphino]-1-methyl-2-phenyl-3H-imidazol-3-ium triflate
• CAS No.: 1253395-50-4
• Molecular Formula: CF₃O₃S*C₂₂H₃₈N₄P
• Molecular Weight: 538.615

Synonyms:3-[bis(diisopropylamino)phosphino]-1-methyl-2-phenyl-3H-imidazol-3-ium triflate

Chemical Property of 3-[bis(diisopropylamino)phosphino]-1-methyl-2-phenyl-3H-imidazol-3-ium triflate

Chemical Property:

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Technology Process of 3-[bis(diisopropylamino)phosphino]-1-methyl-2-phenyl-3H-imidazol-3-ium triflate

There total 1 articles about 3-[bis(diisopropylamino)phosphino]-1-methyl-2-phenyl-3H-imidazol-3-ium triflate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

N-methyl-2-phenyl-1H-imidazole (3475-07-8) + bis(diisopropylamino)phosphenium trifluoromethanesulfonate → 3-[bis(diisopropylamino)phosphino]-1-methyl-2-phenyl-3H-imidazol-3-ium triflate (1253395-50-4)

Guidance literature:

In dichloromethane; at -20 - 20 ℃; Inert atmosphere;

DOI:10.1021/jo101177h

Reference yield: 86.0%

3-[bis(diisopropylamino)phosphino]-1-methyl-2-phenyl-3H-imidazol-3-ium triflate (1253395-50-4) → N,N,N',N'-tetraisopropyl-P-(1-methyl-2-phenyl-1H-imidazol-5-yl)phosphonous diamide (1253395-55-9)

Guidance literature:

With sodium hexamethyldisilazane; In diethyl ether; at -5 - 16 ℃; Inert atmosphere;

DOI:10.1021/jo101177h

upstream raw materials:

N-methyl-2-phenyl-1H-imidazole

Downstream raw materials:

N,N,N',N'-tetraisopropyl-P-(1-methyl-2-phenyl-1H-imidazol-5-yl)phosphonous diamide

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