O-(2,4,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->3)-1,2,4,6-tetra-O-acetyl-β-D-glucopyranose

Base Information

Chemical Name:O-(2,4,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->3)-1,2,4,6-tetra-O-acetyl-β-D-glucopyranose
CAS No.:140420-88-8
Molecular Formula:C₄₁H₄₈O₁₅
Molecular Weight:780.823
Hs Code.:

Synonyms:O-(2,4,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->3)-1,2,4,6-tetra-O-acetyl-β-D-glucopyranose

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Chemical Property of O-(2,4,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->3)-1,2,4,6-tetra-O-acetyl-β-D-glucopyranose

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Technology Process of O-(2,4,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->3)-1,2,4,6-tetra-O-acetyl-β-D-glucopyranose

There total 11 articles about O-(2,4,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->3)-1,2,4,6-tetra-O-acetyl-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 140420-87-7
O-(3-O-allyl-2,4,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->3)-1,2,4,6-tetra-O-acetyl-β-D-glucopyranose

: 140420-88-8
O-(2,4,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->3)-1,2,4,6-tetra-O-acetyl-β-D-glucopyranose

Guidance literature:: With sodium acetate; palladium dichloride; In water; acetic acid; Ambient temperature;
DOI:10.1016/0008-6215(92)84098-D

Reference yield:

: 65877-63-6,97590-76-6,99396-09-5,5531-09-9
3-O-benzyl-D-glucopyranose

: 140420-88-8
O-(2,4,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->3)-1,2,4,6-tetra-O-acetyl-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / pyridine / 0.33 h / Heating

2: 96 percent / H₂, 10percent Pd/C, acetic acid / 760 Torr / Ambient temperature

4: 83 percent / PdCl₂, NaOAc / acetic acid; H₂O / Ambient temperature

With pyridine; palladium on activated charcoal; hydrogen; sodium acetate; acetic acid; palladium dichloride; In water; acetic acid;
DOI:10.1016/0008-6215(92)84098-D

Reference yield:

: 39698-00-5
acetyl 2,4,6-tri-O-acetyl-3-O-allyl-β-D-glucopyranoside

: 140420-88-8
O-(2,4,6-tri-O-benzyl-α-D-glucopyranosyl)-(1->3)-1,2,4,6-tetra-O-acetyl-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 5 steps

1: 82 percent / SnCl₄ / 1,2-dichloro-ethane / 2 h / Ambient temperature

2: 96 percent / M NaOMe / methanol / 1.5 h / Heating

3: 94 percent / NaH, N,N-dimethylformanide / paraffin / 2 h

5: 83 percent / PdCl₂, NaOAc / acetic acid; H₂O / Ambient temperature

With sodium methylate; sodium acetate; tin(IV) chloride; sodium hydride; N,N-dimethyl-formamide; palladium dichloride; In methanol; water; acetic acid; 1,2-dichloro-ethane; paraffin;
DOI:10.1016/0008-6215(92)84098-D