N-(9-{5-hydroxy-4-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-cyclohex-2-enyl}-6-oxo-6,9-dihydro-1H-purin-2-yl)-isobutyramide

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Chemical Name:N-(9-{5-hydroxy-4-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-cyclohex-2-enyl}-6-oxo-6,9-dihydro-1H-purin-2-yl)-isobutyramide
CAS No.:438608-43-6
Molecular Formula:C₃₆H₃₇N₅O₅
Molecular Weight:619.72
Hs Code.:

<i>N</i>-(9-{5-hydroxy-4-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-cyclohex-2-enyl}-6-oxo-6,9-dihydro-1<i>H</i>-purin-2-yl)-isobutyramide

Synonyms:N-(9-{5-hydroxy-4-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-cyclohex-2-enyl}-6-oxo-6,9-dihydro-1H-purin-2-yl)-isobutyramide

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Chemical Property of N-(9-{5-hydroxy-4-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-cyclohex-2-enyl}-6-oxo-6,9-dihydro-1H-purin-2-yl)-isobutyramide

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Technology Process of N-(9-{5-hydroxy-4-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-cyclohex-2-enyl}-6-oxo-6,9-dihydro-1H-purin-2-yl)-isobutyramide

There total 2 articles about N-(9-{5-hydroxy-4-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-cyclohex-2-enyl}-6-oxo-6,9-dihydro-1H-purin-2-yl)-isobutyramide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14470-28-1
mono-4-methoxytrityl chloride

: N-[9-(5-hydroxy-4-hydroxymethyl-cyclohex-2-enyl)-6-oxo-6,9-dihydro-1H-purin-2-yl]-isobutyramide

: 438608-43-6
N-(9-{5-hydroxy-4-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-cyclohex-2-enyl}-6-oxo-6,9-dihydro-1H-purin-2-yl)-isobutyramide

Guidance literature:: With pyridine; at 0 - 20 ℃;
DOI:10.1016/j.tet.2003.12.052

Reference yield:

: 262372-04-3
(1R,4S,5R)-9-(5-hydroxy-4-hydroxymethyl-2-cyclohexen-1-yl)guanine

: 438608-43-6
N-(9-{5-hydroxy-4-[(4-methoxy-phenyl)-diphenyl-methoxymethyl]-cyclohex-2-enyl}-6-oxo-6,9-dihydro-1H-purin-2-yl)-isobutyramide

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / 1 h / 0 °C

1.2: pyridine / 15 h / 0 - 20 °C

1.3: water / 0.25 h / 20 °C

2.1: 420 mg / pyridine / 0 - 20 °C

With pyridine;
DOI:10.1016/j.tet.2003.12.052