Phenylalanyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)serin-methylester

Base Information

Chemical Name:Phenylalanyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)serin-methylester
CAS No.:86041-01-2
Molecular Formula:C₂₇H₃₇N₃O₁₂
Molecular Weight:595.604
Hs Code.:

Synonyms:Phenylalanyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)serin-methylester

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Chemical Property of Phenylalanyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)serin-methylester

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Technology Process of Phenylalanyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)serin-methylester

There total 4 articles about Phenylalanyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)serin-methylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 86040-98-4
N-<2-(Triphenylphosphonio)ethoxycarbonyl>phenylalanyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)serin-methylester-chlorid

: 86041-01-2
Phenylalanyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)serin-methylester

Guidance literature:: With morpholine; In dichloromethane; for 0.333333h; Ambient temperature;
DOI:10.1002/jlac.198319830303

Reference yield:

: 25644-83-1
O-(2-Acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)-N-(benzyloxycarbonyl)serin-methylester

: 86041-01-2
Phenylalanyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)serin-methylester

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / H₂ / 10percent Pd/C / methanol / 3 h / Ambient temperature

2: 81 percent / (ethyl)-2-ethoxy-1,2-dihydro-1-quinolinecarboxylate / CHCl₃ / 1) 1 h, -15 deg C, 2) room temperature, 15 h

3: 80 percent / morpholine / CH₂Cl₂ / 0.33 h / Ambient temperature

With morpholine; hydrogen; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; palladium on activated charcoal; In methanol; dichloromethane; chloroform;
DOI:10.1002/jlac.198319830303

Reference yield:

: 3068-34-6
Acetic acid (2R,3S,4R,5R,6R)-3-acetoxy-2-acetoxymethyl-5-acetylamino-6-chloro-tetrahydro-pyran-4-yl ester

: 86041-01-2
Phenylalanyl-O-(2-acetamido-3,4,6-tri-O-acetyl-2-desoxy-β-D-glucopyranosyl)serin-methylester

Guidance literature:: Multi-step reaction with 4 steps

1: 30 percent / Hg(CN)2 / benzene

2: 94 percent / H₂ / 10percent Pd/C / methanol / 3 h / Ambient temperature

3: 81 percent / (ethyl)-2-ethoxy-1,2-dihydro-1-quinolinecarboxylate / CHCl₃ / 1) 1 h, -15 deg C, 2) room temperature, 15 h

4: 80 percent / morpholine / CH₂Cl₂ / 0.33 h / Ambient temperature

With morpholine; hydrogen; mercury(II) cyanide; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; palladium on activated charcoal; In methanol; dichloromethane; chloroform; benzene;
DOI:10.1002/jlac.198319830303