(2S,1'R)-2-(1'-ethoxymethoxy-3'-methylene-5'-phenylsulfonylpent-1'-yl)tetrahydrofuran

Base Information

• Chemical Name: (2S,1'R)-2-(1'-ethoxymethoxy-3'-methylene-5'-phenylsulfonylpent-1'-yl)tetrahydrofuran
• CAS No.: 1108185-52-9
• Molecular Formula: C₁₉H₂₈O₅S
• Molecular Weight: 368.494

Synonyms:(2S,1'R)-2-(1'-ethoxymethoxy-3'-methylene-5'-phenylsulfonylpent-1'-yl)tetrahydrofuran

Chemical Property of (2S,1'R)-2-(1'-ethoxymethoxy-3'-methylene-5'-phenylsulfonylpent-1'-yl)tetrahydrofuran

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Technology Process of (2S,1'R)-2-(1'-ethoxymethoxy-3'-methylene-5'-phenylsulfonylpent-1'-yl)tetrahydrofuran

There total 1 articles about (2S,1'R)-2-(1'-ethoxymethoxy-3'-methylene-5'-phenylsulfonylpent-1'-yl)tetrahydrofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

C19H28O3S (1108185-80-3) → (2S,1'R)-2-(1'-ethoxymethoxy-3'-methylene-5'-phenylsulfonylpent-1'-yl)tetrahydrofuran (1108185-52-9)

Guidance literature:

With aluminum oxide; Oxone; In chloroform; at 20 ℃; for 3h; Reflux;

DOI:10.1021/ol8025457

Reference yield: 91.0%

(2R,5R,2'R)-5-(formyl)-2-[3'-(4-methoxybenzyloxy)-2'-methylpropyl]-2-methyltetrahydrofuran (1108185-46-1) + (2S,1'R)-2-(1'-ethoxymethoxy-3'-methylene-5'-phenylsulfonylpent-1'-yl)tetrahydrofuran (1108185-52-9) → C37H54O9S (1108185-82-5)

Guidance literature:

(2S,1'R)-2-(1'-ethoxymethoxy-3'-methylene-5'-phenylsulfonylpent-1'-yl)tetrahydrofuran; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.5h; Inert atmosphere;

(2R,5R,2'R)-5-(formyl)-2-[3'-(4-methoxybenzyloxy)-2'-methylpropyl]-2-methyltetrahydrofuran; In tetrahydrofuran; at -78 ℃; Inert atmosphere;

DOI:10.1021/ol8025457

upstream raw materials:

C₁₉H₂₈O₃S

Downstream raw materials:

C₃₇H₅₄O₉S

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