7-Benzyloxy-1-(5-benzyloxy-2-bromo-4-methoxy-benzyl)-8-bromo-6-methoxy-3,4-dihydro-isoquinoline

Base Information

Chemical Name:7-Benzyloxy-1-(5-benzyloxy-2-bromo-4-methoxy-benzyl)-8-bromo-6-methoxy-3,4-dihydro-isoquinoline
CAS No.:86639-20-5
Molecular Formula:C₃₂H₂₉Br₂NO₄
Molecular Weight:651.395
Hs Code.:

Synonyms:7-Benzyloxy-1-(5-benzyloxy-2-bromo-4-methoxy-benzyl)-8-bromo-6-methoxy-3,4-dihydro-isoquinoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 7-Benzyloxy-1-(5-benzyloxy-2-bromo-4-methoxy-benzyl)-8-bromo-6-methoxy-3,4-dihydro-isoquinoline

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 7-Benzyloxy-1-(5-benzyloxy-2-bromo-4-methoxy-benzyl)-8-bromo-6-methoxy-3,4-dihydro-isoquinoline

There total 5 articles about 7-Benzyloxy-1-(5-benzyloxy-2-bromo-4-methoxy-benzyl)-8-bromo-6-methoxy-3,4-dihydro-isoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 38849-47-7
2-(5-Benzyloxy-2-bromo-4-methoxy-phenyl)-N-[2-(4-benzyloxy-3-bromo-5-methoxy-phenyl)-ethyl]-acetamide

: 86639-20-5
7-Benzyloxy-1-(5-benzyloxy-2-bromo-4-methoxy-benzyl)-8-bromo-6-methoxy-3,4-dihydro-isoquinoline

Guidance literature:: With trichlorophosphate; In benzene; for 2h; Heating;

Reference yield:

: 35320-87-7,54737-26-7
4-benzyloxy-5-bromo-3-methoxy-ω-nitrostyrene

: 86639-20-5
7-Benzyloxy-1-(5-benzyloxy-2-bromo-4-methoxy-benzyl)-8-bromo-6-methoxy-3,4-dihydro-isoquinoline

Guidance literature:: Multi-step reaction with 4 steps

1: 52.8 percent / NaBH₄ / methanol / 2 h / Ambient temperature

2: 82.7 percent / hydrazine hydrate / Raney-Ni / ethanol / 1 h / Ambient temperature

3: 78 percent / benzene / 3 h / Ambient temperature

4: 82 percent / POCl₃ / benzene / 2 h / Heating

With sodium tetrahydroborate; hydrazine hydrate; trichlorophosphate; nickel; In methanol; ethanol; benzene;

Reference yield:

: 86639-26-1
α-<4-benzyloxy-5-bromo-3-methoxyphenyl>β-nitroethane

: 86639-20-5
7-Benzyloxy-1-(5-benzyloxy-2-bromo-4-methoxy-benzyl)-8-bromo-6-methoxy-3,4-dihydro-isoquinoline

Guidance literature:: Multi-step reaction with 3 steps

1: 82.7 percent / hydrazine hydrate / Raney-Ni / ethanol / 1 h / Ambient temperature

2: 78 percent / benzene / 3 h / Ambient temperature

3: 82 percent / POCl₃ / benzene / 2 h / Heating

With hydrazine hydrate; trichlorophosphate; nickel; In ethanol; benzene;