(2R,3R,4R,5S,6R)-3,4,5-tris(benzyloxy)-2-((benzyloxy)methyl)-6-phenyltetrahydro-2H-pyran

Base Information

Chemical Name:(2R,3R,4R,5S,6R)-3,4,5-tris(benzyloxy)-2-((benzyloxy)methyl)-6-phenyltetrahydro-2H-pyran
CAS No.:116417-38-0
Molecular Formula:C₄₀H₄₀O₅
Molecular Weight:600.755
Hs Code.:

Synonyms:(2R,3R,4R,5S,6R)-3,4,5-tris(benzyloxy)-2-((benzyloxy)methyl)-6-phenyltetrahydro-2H-pyran

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Chemical Property of (2R,3R,4R,5S,6R)-3,4,5-tris(benzyloxy)-2-((benzyloxy)methyl)-6-phenyltetrahydro-2H-pyran

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Technology Process of (2R,3R,4R,5S,6R)-3,4,5-tris(benzyloxy)-2-((benzyloxy)methyl)-6-phenyltetrahydro-2H-pyran

There total 8 articles about (2R,3R,4R,5S,6R)-3,4,5-tris(benzyloxy)-2-((benzyloxy)methyl)-6-phenyltetrahydro-2H-pyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 591-50-4
iodobenzene

: (2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl)tri-n-butylstannane

: 116417-38-0
(2R,3R,4R,5S,6R)-3,4,5-tris(benzyloxy)-2-((benzyloxy)methyl)-6-phenyltetrahydro-2H-pyran

Guidance literature:: With potassium fluoride; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; C₅₁H₇₃O₂P; copper(l) chloride; In m-xylene; at 140 ℃; for 72h; Inert atmosphere;
DOI:10.1021/jacs.6b07891

Reference yield: 40.0%

: 25320-59-6
tetra-O-benzyl glucopyranosyl chloride

: phenylzinc iodide-lithium chloride complex

: 95839-12-6
D-Glucopyranosyl-benzol

: 112219-64-4
(2R,3R,4R,5S,6S)-3,4,5-tris(benzyloxy)-2-((benzyloxy)methyl)-6-phenyltetrahydro-2H-pyran

: 116417-38-0
(2R,3R,4R,5S,6R)-3,4,5-tris(benzyloxy)-2-((benzyloxy)methyl)-6-phenyltetrahydro-2H-pyran

Guidance literature:: With bis (1,5-cyclopentadiene)nickel ⁽⁰⁾; 4,4',4-tri-tert-butyl-2,2':6',2-terpyridine; In N,N-dimethyl-formamide; at 25 ℃; for 12h; optical yield given as %de;
DOI:10.1021/ja8041564

Reference yield:

: 38184-10-0
phenyl 2,3,4,5-tetra-O-benzyl-1-thio-β-D-glucopyranoside

: 1078-58-6
diphenylzinc

: 112219-64-4
(2R,3R,4R,5S,6S)-3,4,5-tris(benzyloxy)-2-((benzyloxy)methyl)-6-phenyltetrahydro-2H-pyran

: 116417-38-0
(2R,3R,4R,5S,6R)-3,4,5-tris(benzyloxy)-2-((benzyloxy)methyl)-6-phenyltetrahydro-2H-pyran

Guidance literature:: With diiodomethane; In toluene; at 50 ℃; for 2h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1016/S0008-6215(00)90882-6