(dimethyl(phenyl)silyl)-[D₂]methyl 2,2,6,6-tetramethylpiperidine-1-carboxylate

Base Information

Chemical Name:(dimethyl(phenyl)silyl)-[D₂]methyl 2,2,6,6-tetramethylpiperidine-1-carboxylate
CAS No.:1051942-95-0
Molecular Formula:C₁₉H₃₁NO₂Si
Molecular Weight:335.53
Hs Code.:

(dimethyl(phenyl)silyl)-[D<sub>2</sub>]methyl 2,2,6,6-tetramethylpiperidine-1-carboxylate

Synonyms:(dimethyl(phenyl)silyl)-[D₂]methyl 2,2,6,6-tetramethylpiperidine-1-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (dimethyl(phenyl)silyl)-[D₂]methyl 2,2,6,6-tetramethylpiperidine-1-carboxylate

Chemical Property:

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Technology Process of (dimethyl(phenyl)silyl)-[D₂]methyl 2,2,6,6-tetramethylpiperidine-1-carboxylate

There total 2 articles about (dimethyl(phenyl)silyl)-[D₂]methyl 2,2,6,6-tetramethylpiperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 1051943-03-3
[D₃]methyl 2,2,6,6-tetramethylpiperidine-1-carboxylate

: 768-33-2
phenyldimethylsilyl chloride

: 1051942-95-0
(dimethyl(phenyl)silyl)-[D₂]methyl 2,2,6,6-tetramethylpiperidine-1-carboxylate

Guidance literature:: [D₃]methyl 2,2,6,6-tetramethylpiperidine-1-carboxylate; With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; In diethyl ether; cyclohexane; at -78 ℃; for 72h;

phenyldimethylsilyl chloride; In diethyl ether; cyclohexane; at -78 - 20 ℃; for 18h; Further stages.;
DOI:10.1016/j.tet.2008.05.091

Reference yield:

: 1051943-04-4
[D₂]methyl 2,2,6,6-tetramethylpiperidine-1-carboxylate

: 768-33-2
phenyldimethylsilyl chloride

: 1051942-95-0
(dimethyl(phenyl)silyl)-[D₂]methyl 2,2,6,6-tetramethylpiperidine-1-carboxylate

: C₁₉H₃₀⁽²⁾HNO₂Si

Guidance literature:: [D₂]methyl 2,2,6,6-tetramethylpiperidine-1-carboxylate; With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; In diethyl ether; cyclohexane; at -78 ℃; for 18h;

phenyldimethylsilyl chloride; In diethyl ether; cyclohexane; at -78 - 20 ℃; for 3h; Further stages. Title compound not separated from byproducts.;
DOI:10.1016/j.tet.2008.05.091

Reference yield: 47.0%

: 869218-52-0
(R,R)-1,2-dicyclohexylethane-1,2-diol tert-butyl alcohol borate

: 1051942-95-0
(dimethyl(phenyl)silyl)-[D₂]methyl 2,2,6,6-tetramethylpiperidine-1-carboxylate

: 1051943-07-7
C₃₃H₅₃⁽²⁾HBNO₄Si

: 1051943-06-6
C₃₃H₅₃⁽²⁾HBNO₄Si

Guidance literature:: (dimethyl(phenyl)silyl)-[D₂]methyl 2,2,6,6-tetramethylpiperidine-1-carboxylate; With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; In diethyl ether; cyclohexane; at -78 ℃; for 1h;

(R,R)-1,2-dicyclohexylethane-1,2-diol tert-butyl alcohol borate; In diethyl ether; cyclohexane; at -78 ℃; for 1h; Further stages.;
DOI:10.1016/j.tet.2008.05.091