methyl-2-O-benzyl-3-O-(4,6-O-benzylidene-2-deoxy-β-D-arabino-hexopyranosyl)-6-deoxy-4-O-methyl-β-D-galactopyranoside

Base Information

Chemical Name:methyl-2-O-benzyl-3-O-(4,6-O-benzylidene-2-deoxy-β-D-arabino-hexopyranosyl)-6-deoxy-4-O-methyl-β-D-galactopyranoside
CAS No.:129081-08-9
Molecular Formula:C₂₈H₃₆O₉
Molecular Weight:516.588
Hs Code.:

Synonyms:methyl-2-O-benzyl-3-O-(4,6-O-benzylidene-2-deoxy-β-D-arabino-hexopyranosyl)-6-deoxy-4-O-methyl-β-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl-2-O-benzyl-3-O-(4,6-O-benzylidene-2-deoxy-β-D-arabino-hexopyranosyl)-6-deoxy-4-O-methyl-β-D-galactopyranoside

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Technology Process of methyl-2-O-benzyl-3-O-(4,6-O-benzylidene-2-deoxy-β-D-arabino-hexopyranosyl)-6-deoxy-4-O-methyl-β-D-galactopyranoside

There total 2 articles about methyl-2-O-benzyl-3-O-(4,6-O-benzylidene-2-deoxy-β-D-arabino-hexopyranosyl)-6-deoxy-4-O-methyl-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1125-88-8
benzaldehyde dimethyl acetal

: 129081-07-8
methyl 2-O-benzyl-6-deoxy-3-O-(2-deoxy-β-D-arabino-hexopyranosyl)-4-O-methyl-β-D-galactopyranoside

: 129081-08-9
methyl-2-O-benzyl-3-O-(4,6-O-benzylidene-2-deoxy-β-D-arabino-hexopyranosyl)-6-deoxy-4-O-methyl-β-D-galactopyranoside

Guidance literature:: With camphor-10-sulfonic acid; In N,N-dimethyl-formamide; at 80 ℃; for 3h; under 52.5 Torr;
DOI:10.1016/0008-6215(90)84084-8

Reference yield:

: 125084-98-2
methyl 2-O-benzyl-6-deoxy-4-O-methyl-3-O-(3,4,6-tri-O-acetyl-2-deoxy-β-D-arabino-hexapyranosyl)-β-D-galactopyranoside

: 129081-08-9
methyl-2-O-benzyl-3-O-(4,6-O-benzylidene-2-deoxy-β-D-arabino-hexopyranosyl)-6-deoxy-4-O-methyl-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / NaOCH₃ / methanol / 1.5 h / Ambient temperature

2: 96 percent / (+/-)-camphor-10-sulfonic acid / dimethylformamide / 3 h / 80 °C / 52.5 Torr

With camphor-10-sulfonic acid; sodium methylate; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(90)84084-8

Reference yield: 89.0%

: 129081-08-9
methyl-2-O-benzyl-3-O-(4,6-O-benzylidene-2-deoxy-β-D-arabino-hexopyranosyl)-6-deoxy-4-O-methyl-β-D-galactopyranoside

: 129081-09-0
methyl-2-O-benzyl-3-O-(4,6-O-benzylidene-2-deoxy-β-D-erythro-hexopyranosyl-3-ulose)-6-deoxy-4-O-methyl-β-D-galactopyranoside

Guidance literature:: With 4 A molecular sieve; pyridinium chlorochromate; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1016/0008-6215(90)84084-8