S-phenyl α-bromothiopropionate

Base Information

• Chemical Name: S-phenyl α-bromothiopropionate
• CAS No.: 120346-72-7
• Molecular Formula: C₉H₉BrOS
• Molecular Weight: 245.14

Synonyms:S-phenyl α-bromothiopropionate

Chemical Property of S-phenyl α-bromothiopropionate

Chemical Property:

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Technology Process of S-phenyl α-bromothiopropionate

There total 8 articles about S-phenyl α-bromothiopropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

thiophenol (108-98-5) + α-bromopropionyl bromide (563-76-8) → S-phenyl α-bromothiopropionate (120346-72-7)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; for 0.5h;

DOI:10.1021/ol102407k

Reference yield: 73.0%

(E)-3-methyl-2-phenylsulphonyl-2-phenylthiooxirane (120346-61-4) → S-phenyl α-bromothiopropionate (120346-72-7)

Guidance literature:

With magnesium bromide; In diethyl ether; at 20 ℃; for 6h;

DOI:10.1016/S0040-4039(00)80635-8

Reference yield: 40.0%

thiophenol (108-98-5) + 2-Bromopropionyl chloride (7148-74-5) → S-phenyl α-bromothiopropionate (120346-72-7)

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃;

DOI:10.1021/ol990971n

upstream raw materials:

(E)-3-methyl-2-phenylsulphonyl-2-phenylthiooxirane

propionic acid

thiophenol

2-Bromopropionyl chloride

Downstream raw materials:

S-phenyl α-iodothiopropionate

2-(triphenylphosphoranylidene)propanethioic acid S-phenyl ester

S-phenyl 2-hydroxy(thiopropanoate)

anti-S-phenyl 3-hydroxy-2-methyl-3-phenylpropanethioate

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