rac-(SiR,CS/SiS,CR)-t-butylmethyl-<1-(3,5-dinitrobenzoyloxy)ethyl>phenylsilane

Base Information

Chemical Name:rac-(SiR,CS/SiS,CR)-t-butylmethyl-<1-(3,5-dinitrobenzoyloxy)ethyl>phenylsilane
CAS No.:133858-10-3
Molecular Formula:C₂₀H₂₄N₂O₆Si
Molecular Weight:416.506
Hs Code.:

Synonyms:rac-(SiR,CS/SiS,CR)-t-butylmethyl-<1-(3,5-dinitrobenzoyloxy)ethyl>phenylsilane

Suppliers and Price of rac-(SiR,CS/SiS,CR)-t-butylmethyl-<1-(3,5-dinitrobenzoyloxy)ethyl>phenylsilane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of rac-(SiR,CS/SiS,CR)-t-butylmethyl-<1-(3,5-dinitrobenzoyloxy)ethyl>phenylsilane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of rac-(SiR,CS/SiS,CR)-t-butylmethyl-<1-(3,5-dinitrobenzoyloxy)ethyl>phenylsilane

There total 2 articles about rac-(SiR,CS/SiS,CR)-t-butylmethyl-<1-(3,5-dinitrobenzoyloxy)ethyl>phenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 99-34-3
3,5-dinitrobenzoic acid

: 133858-07-8,133858-08-9,133907-51-4,133907-52-5
rac-(SiR,CS/SiS,CR)-t-butyl(1-hydroxyethyl)methylphenylsilane

: 133858-10-3
rac-(SiR,CS/SiS,CR)-t-butylmethyl-<1-(3,5-dinitrobenzoyloxy)ethyl>phenylsilane

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 48h; Ambient temperature;
DOI:10.1016/0022-328X(91)83084-H

Reference yield:

: 129340-98-3
rac-acetyl(t-butyl)methylphenylsilane

: 133858-10-3
rac-(SiR,CS/SiS,CR)-t-butylmethyl-<1-(3,5-dinitrobenzoyloxy)ethyl>phenylsilane

Guidance literature:: Multi-step reaction with 2 steps

1: 42 percent / LiAlH₄ / diethyl ether / 2 h / Ambient temperature

2: 93 percent / N,N'-dicyclokexylcarbodiimide, 4-(dimethylamino)pyridine / CH₂Cl₂ / 48 h / Ambient temperature

With dmap; lithium aluminium tetrahydride; dicyclohexyl-carbodiimide; In diethyl ether; dichloromethane;
DOI:10.1016/0022-328X(91)83084-H