7-[4-(3-azido-5-azidomethylbenzyloxy)phenylcarbamoyl]heptananoic acid methyl ester

Base Information

Chemical Name:7-[4-(3-azido-5-azidomethylbenzyloxy)phenylcarbamoyl]heptananoic acid methyl ester
CAS No.:1197892-26-4
Molecular Formula:C₂₃H₂₇N₇O₄
Molecular Weight:465.512
Hs Code.:

Synonyms:7-[4-(3-azido-5-azidomethylbenzyloxy)phenylcarbamoyl]heptananoic acid methyl ester

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Chemical Property of 7-[4-(3-azido-5-azidomethylbenzyloxy)phenylcarbamoyl]heptananoic acid methyl ester

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Technology Process of 7-[4-(3-azido-5-azidomethylbenzyloxy)phenylcarbamoyl]heptananoic acid methyl ester

There total 5 articles about 7-[4-(3-azido-5-azidomethylbenzyloxy)phenylcarbamoyl]heptananoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1197892-23-1
7-(4-hydroxyphenylcarbamoyl)heptananoic acid methyl ester

: 849607-13-2
methanesulfonic acid 3-azido-5-azidomethyl-benzyl ester

: 1197892-26-4
7-[4-(3-azido-5-azidomethylbenzyloxy)phenylcarbamoyl]heptananoic acid methyl ester

Guidance literature:: With potassium carbonate; In acetone; at 20 ℃; for 12h;
DOI:10.1021/jm9005077

Reference yield:

: 3946-32-5
suberic acid monomethyl ester

: 1197892-26-4
7-[4-(3-azido-5-azidomethylbenzyloxy)phenylcarbamoyl]heptananoic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C

2: palladium 10% on activated carbon; methanol / 20 °C

3: potassium carbonate / acetone / Reflux

With methanol; palladium 10% on activated carbon; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; acetone;
DOI:10.1016/j.bmcl.2012.08.104

Reference yield:

: 1197892-22-0
7-(4-benzyloxyphenylcarbamoyl)heptananoic acid methyl ester

: 1197892-26-4
7-[4-(3-azido-5-azidomethylbenzyloxy)phenylcarbamoyl]heptananoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; methanol / 20 °C

2: potassium carbonate / acetone / Reflux

With methanol; palladium 10% on activated carbon; potassium carbonate; In acetone;
DOI:10.1016/j.bmcl.2012.08.104