C₂₈H₂₇F₂NO₇S

Base Information

Chemical Name:C₂₈H₂₇F₂NO₇S
CAS No.:1374235-15-0
Molecular Formula:C₂₈H₂₇F₂NO₇S
Molecular Weight:559.588
Hs Code.:

C<sub>28</sub>H<sub>27</sub>F<sub>2</sub>NO<sub>7</sub>S

Synonyms:C₂₈H₂₇F₂NO₇S

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Chemical Property of C₂₈H₂₇F₂NO₇S

Chemical Property:

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Technology Process of C₂₈H₂₇F₂NO₇S

There total 7 articles about C₂₈H₂₇F₂NO₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1374235-14-9
C₂₈H₂₅F₂NO₇S

: 1374235-15-0
C₂₈H₂₇F₂NO₇S

Guidance literature:: C₂₈H₂₅F₂NO₇S; With sodium tetrahydroborate; In tetrahydrofuran; ethanol; at 0 - 20 ℃; for 2h;

With water;

Reference yield:

: 691857-46-2
ethyl 2-(4-fluorophenyl)-5-hydroxy-6-nitrobenzofuran-3-carboxylate

: 1374235-15-0
C₂₈H₂₇F₂NO₇S

Guidance literature:: Multi-step reaction with 8 steps

1.1: N-ethyl-N,N-diisopropylamine / dmap / dichloromethane / 2 h / 0 °C

2.1: triethylamine / (diphenylphosphin)ferrocene; palladium diacetate / N,N-dimethyl-formamide / 2 h / 100 °C / Inert atmosphere

3.1: hydrogenchloride; water / tetrahydrofuran / 0.25 h / 20 °C

4.1: tin(II) chloride dihdyrate / ethyl acetate / 1 h / 80 °C

4.2: 0.5 h / 20 °C

5.1: pyridine / 1 h / 0 - 20 °C

6.1: sodium tetrahydroborate / ethanol; dichloromethane / 2 h / 0 °C

7.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 50 °C

8.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 2 h / 0 - 20 °C

With pyridine; hydrogenchloride; sodium tetrahydroborate; tin(II) chloride dihdyrate; water; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; dmap; (diphenylphosphin)ferrocene; palladium diacetate; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 691857-07-5
ethyl 2-(4-fluorophenyl)-5-isopropoxy-6-nitrobenzofuran-3-carboxylate

: 1374235-15-0
C₂₈H₂₇F₂NO₇S

Guidance literature:: Multi-step reaction with 9 steps

1.1: boron trichloride / dichloromethane / 1 h / 0 - 20 °C

1.2: Cooling with ice

2.1: N-ethyl-N,N-diisopropylamine / dmap / dichloromethane / 2 h / 0 °C

3.1: triethylamine / (diphenylphosphin)ferrocene; palladium diacetate / N,N-dimethyl-formamide / 2 h / 100 °C / Inert atmosphere

4.1: hydrogenchloride; water / tetrahydrofuran / 0.25 h / 20 °C

5.1: tin(II) chloride dihdyrate / ethyl acetate / 1 h / 80 °C

5.2: 0.5 h / 20 °C

6.1: pyridine / 1 h / 0 - 20 °C

7.1: sodium tetrahydroborate / ethanol; dichloromethane / 2 h / 0 °C

8.1: potassium carbonate / N,N-dimethyl-formamide / 2 h / 50 °C

9.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 2 h / 0 - 20 °C

With pyridine; hydrogenchloride; sodium tetrahydroborate; tin(II) chloride dihdyrate; water; boron trichloride; potassium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; dmap; (diphenylphosphin)ferrocene; palladium diacetate; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;