C₄₉H₆₉NO₉

Base Information

• Chemical Name: C₄₉H₆₉NO₉
• CAS No.: 1307870-88-7
• Molecular Formula: C₄₉H₆₉NO₉
• Molecular Weight: 816.088
• Mol file: 1307870-88-7.mol

Synonyms:C₄₉H₆₉NO₉

Chemical Property of C₄₉H₆₉NO₉

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₉H₆₉NO₉

There total 9 articles about C₄₉H₆₉NO₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

C25H34O7S (1307870-93-4) + solasodine (126-17-0) → C49H69NO9 (1307870-88-7)

Guidance literature:

With N-iodo-succinimide; silver trifluoromethanesulfonate; at -50 ℃; for 2h;

DOI:10.1016/j.bmcl.2011.03.064

Reference yield:

C43H59N3O3Si (1307870-96-7) → C49H69NO9 (1307870-88-7)

Guidance literature:

Multi-step reaction with 4 steps

1: sodium tetrahydroborate / isopropyl alcohol / 5 h / 20 °C

2: triphenylphosphine / tetrahydrofuran; water / 6 h / Reflux

3: hydrogenchloride; water / ethanol / 2 h / Reflux

4: N-iodo-succinimide; silver trifluoromethanesulfonate / 2 h / -50 °C

With hydrogenchloride; sodium tetrahydroborate; N-iodo-succinimide; water; silver trifluoromethanesulfonate; triphenylphosphine; In tetrahydrofuran; ethanol; water; isopropyl alcohol;

DOI:10.1016/j.bmcl.2011.03.064

Reference yield:

C43H61N3O3Si (1307870-98-9) → C49H69NO9 (1307870-88-7)

Guidance literature:

Multi-step reaction with 3 steps

1: triphenylphosphine / tetrahydrofuran; water / 6 h / Reflux

2: hydrogenchloride; water / ethanol / 2 h / Reflux

3: N-iodo-succinimide; silver trifluoromethanesulfonate / 2 h / -50 °C

With hydrogenchloride; N-iodo-succinimide; water; silver trifluoromethanesulfonate; triphenylphosphine; In tetrahydrofuran; ethanol; water;

DOI:10.1016/j.bmcl.2011.03.064

upstream raw materials:

C₄₃H₅₉N₃O₃Si

C₄₃H₆₁N₃O₃Si

C₂₅H₃₄O₇S

solasodine

Downstream raw materials:

C₇₃H₁₀₁NO₂₃