Technology Process of C31H31N5O7S3
There total 5 articles about C31H31N5O7S3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane;
at 20 ℃;
for 12h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium azide / water; acetone / 3 h / 20 °C
2: potassium carbonate / acetonitrile; water / 12 h / 20 °C
3: potassium carbonate / acetonitrile; water / 24 h / Reflux
4: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 12 h / 20 °C
With
dmap; sodium azide; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane; water; acetone; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: p-toluenemethanesulfonic acid / benzene / 10 h / Reflux
2: potassium carbonate / acetonitrile; water / 24 h / Reflux
3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 12 h / 20 °C
With
dmap; p-toluenemethanesulfonic acid; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride;
In
dichloromethane; water; acetonitrile; benzene;