trismethyluranium

Base Information

Chemical Name:trismethyluranium
CAS No.:69517-44-8
Molecular Formula:C₁₉H₅₇N₃Si₆U
Molecular Weight:734.224
Hs Code.:

tris<bis(trimethylsilyl)amido>methyluranium

Synonyms:trismethyluranium

Suppliers and Price of trismethyluranium

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of trismethyluranium

Chemical Property:

Purity/Quality:

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Technology Process of trismethyluranium

There total 1 articles about trismethyluranium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1286281-71-7
U(H₂C=PPh₃)[N(SiMe₃)2]3

: U(IV)(bis(trimethylsilyl)amido)3(CHPPh₃)

: 69517-44-8
trismethyluranium

Guidance literature:: With 2,2,6,6-tetramethylpiperidine-1-oxyl; In benzene-d6; byproducts: P(C6H5)3, tetramethylpiperidine; addn. of piperidineoxyl deriv. to C6D6 soln. of uranium compd. at room temp., keeping for 2.5 h; NMR monitoring;
DOI:10.1021/ja2001133

Reference yield: 80.0%

: 69517-44-8
trismethyluranium

: 103-79-7,136675-26-8
1-phenyl-acetone

: 107145-76-6
(((CH₃)3Si)2N)3UOC(CH₃)2(CH₂C₆H₅)

Guidance literature:: In benzene; uranium compd. is dissolved in benzene, phenyl-2-propanone is added at 0°C, stirring for 12 h; evapn., extn. (pentane), concn., cooling to -70°C;
DOI:10.1016/S0022-328X(00)99792-4

Reference yield: 77.0%

: 931-53-3
Cyclohexyl isocyanide

: 69517-44-8
trismethyluranium

: 113678-08-3
((Si(CH₃)3)2N)3U(CN(C₆H₁₁))CH₃

Guidance literature:: In pentane; uranium compd. is dissolved in pentane, cyclohexylisonitrile is added at 0°C, stirring 1 h; evapn., residue extd., concn., cooling;
DOI:10.1016/S0022-328X(00)99792-4