C₅₉H₅₃Cl₄N₇O₁₄

Base Information

Chemical Name:C₅₉H₅₃Cl₄N₇O₁₄
CAS No.:586413-58-3
Molecular Formula:C₅₉H₅₃Cl₄N₇O₁₄
Molecular Weight:1225.92
Hs Code.:

C<sub>59</sub>H<sub>53</sub>Cl<sub>4</sub>N<sub>7</sub>O<sub>14</sub>

Synonyms:C₅₉H₅₃Cl₄N₇O₁₄

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Chemical Property of C₅₉H₅₃Cl₄N₇O₁₄

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Technology Process of C₅₉H₅₃Cl₄N₇O₁₄

There total 26 articles about C₅₉H₅₃Cl₄N₇O₁₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: C₆₂H₆₂Cl₄IN₇O₁₄Sn

: 586413-58-3
C₅₉H₅₃Cl₄N₇O₁₄

Guidance literature:: With 2,3,5-trimethyl-pyridine; bis(tri-t-butylphosphine)palladium⁽⁰⁾; cesium fluoride; In 1,4-dioxane; at 50 ℃; for 5h;
DOI:10.1021/ja030249r

Reference yield:

: 621-59-0
isovanillin

: 586413-58-3
C₅₉H₅₃Cl₄N₇O₁₄

Guidance literature:: Multi-step reaction with 15 steps

1: 98 percent / imidazole / dimethylformamide / 0.5 h

2: 98 percent / MgSO₄ / benzene / 24 h

3: Ti(O-i-Pr)4; chiral amino acid ligand; isopropanol / toluene / 4 h

4: 3.11 g / NaHCO₃; 1-hydroxy-7-azabenzotriazole; 1-[3-(dimethylamino)propyl]-3-ethylcarbodiimide / tetrahydrofuran; dimethylformamide / 12 h / 22 °C

5: NH₄OAc; aq. NaIO₄ / acetone / 12 h / 22 °C

6: 650 mg / Cu(OAc)2; 4A molecular sieves; Et₃N / CH₂Cl₂; methanol / 6 h / 22 °C

7: 98 percent / HCl / methanol / 1.5 h / 22 °C

8: 860 mg / 2,6-lutidine / CH₂Cl₂ / 2 h

9: 1.0 g / AlBr₃; EtSH / 1.5 h / 0 °C

10: 940 mg / 1-hydroxy-7-azabenzotriazole; 1-[3-(dimethylamino)propyl]-3-ethylcarbodiimide; NaHCO₃ / tetrahydrofuran / 12 h / 22 °C

11: 390 mg / NIS / acetonitrile / 0.42 h / 22 °C

12: 85 mg / HCl / methanol / 5 h / 45 °C

13: 98 mg / HATU; collidine / tetrahydrofuran; CH₂Cl₂ / 3 h / 0 - 22 °C

With 1H-imidazole; 2,6-dimethylpyridine; titanium(IV) isopropylate; 2,3,5-trimethyl-pyridine; hydrogenchloride; sodium periodate; N-iodo-succinimide; 1-hydroxy-7-aza-benzotriazole; aluminum tri-bromide; copper diacetate; 4 A molecular sieve; chiral amino acid ligand; ammonium acetate; sodium hydrogencarbonate; magnesium sulfate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; isopropyl alcohol; ethanethiol; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetone; toluene; acetonitrile; benzene;
DOI:10.1021/ja030249r

Reference yield:

: 97315-18-9
p-methoxy-m-(tert-butyldimethylsilyloxy)-benzaldehyde

: 586413-58-3
C₅₉H₅₃Cl₄N₇O₁₄

Guidance literature:: Multi-step reaction with 14 steps

1: 98 percent / MgSO₄ / benzene / 24 h

2: Ti(O-i-Pr)4; chiral amino acid ligand; isopropanol / toluene / 4 h

3: 3.11 g / NaHCO₃; 1-hydroxy-7-azabenzotriazole; 1-[3-(dimethylamino)propyl]-3-ethylcarbodiimide / tetrahydrofuran; dimethylformamide / 12 h / 22 °C

4: NH₄OAc; aq. NaIO₄ / acetone / 12 h / 22 °C

5: 650 mg / Cu(OAc)2; 4A molecular sieves; Et₃N / CH₂Cl₂; methanol / 6 h / 22 °C

6: 98 percent / HCl / methanol / 1.5 h / 22 °C

7: 860 mg / 2,6-lutidine / CH₂Cl₂ / 2 h

8: 1.0 g / AlBr₃; EtSH / 1.5 h / 0 °C

9: 940 mg / 1-hydroxy-7-azabenzotriazole; 1-[3-(dimethylamino)propyl]-3-ethylcarbodiimide; NaHCO₃ / tetrahydrofuran / 12 h / 22 °C

10: 390 mg / NIS / acetonitrile / 0.42 h / 22 °C

11: 85 mg / HCl / methanol / 5 h / 45 °C

12: 98 mg / HATU; collidine / tetrahydrofuran; CH₂Cl₂ / 3 h / 0 - 22 °C

With 2,6-dimethylpyridine; titanium(IV) isopropylate; 2,3,5-trimethyl-pyridine; hydrogenchloride; sodium periodate; N-iodo-succinimide; 1-hydroxy-7-aza-benzotriazole; aluminum tri-bromide; copper diacetate; 4 A molecular sieve; chiral amino acid ligand; ammonium acetate; sodium hydrogencarbonate; magnesium sulfate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; isopropyl alcohol; ethanethiol; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetone; toluene; acetonitrile; benzene;
DOI:10.1021/ja030249r