ethyl 1-benzyl-9-methoxy-3-methyl-1H-benzindole-2-carboxylate

Base Information

Chemical Name:ethyl 1-benzyl-9-methoxy-3-methyl-1H-benzindole-2-carboxylate
CAS No.:151646-85-4
Molecular Formula:C₂₄H₂₃NO₃
Molecular Weight:373.452
Hs Code.:

ethyl 1-benzyl-9-methoxy-3-methyl-1H-benz<f>indole-2-carboxylate

Synonyms:ethyl 1-benzyl-9-methoxy-3-methyl-1H-benzindole-2-carboxylate

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Chemical Property of ethyl 1-benzyl-9-methoxy-3-methyl-1H-benzindole-2-carboxylate

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Technology Process of ethyl 1-benzyl-9-methoxy-3-methyl-1H-benzindole-2-carboxylate

There total 1 articles about ethyl 1-benzyl-9-methoxy-3-methyl-1H-benzindole-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 151646-84-3
ethyl 1-benzyl-3-methyl-9-oxo-4,9-dihydro-1H-benzindole-2-carboxylate

: 77-78-1
dimethyl sulfate

: 151646-85-4
ethyl 1-benzyl-9-methoxy-3-methyl-1H-benzindole-2-carboxylate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 0 ℃; for 0.333333h;
DOI:10.1002/jhet.5570300137

Reference yield:

: 151646-85-4
ethyl 1-benzyl-9-methoxy-3-methyl-1H-benzindole-2-carboxylate

: 1026976-54-4
1-benzyl-9-methoxy-3-methyl-1H-benzindole-2-carboxylic acid

Guidance literature:: With potassium hydroxide; In ethanol; for 0.75h; Heating;
DOI:10.1002/jhet.5570300137

Reference yield:

: 151646-85-4
ethyl 1-benzyl-9-methoxy-3-methyl-1H-benzindole-2-carboxylate

: 1-benzyl-9-methoxy-3-methyl-5,6,7,8-tetrahydro-1H-benzindole

Guidance literature:: Multi-step reaction with 3 steps

1: KOH / ethanol / 0.75 h / Heating

2: copper chromite / quinoline / 0.25 h / 200 °C

3: 73 percent / Raney Ni-W₄ / ethanol / 1.5 h / Heating

With potassium hydroxide; copper chromite; Raney Ni-W₄; In quinoline; ethanol;
DOI:10.1002/jhet.5570300137