bis-(4-benzyloxy-butyl)-sulfide

Base Information

• Chemical Name: bis-(4-benzyloxy-butyl)-sulfide
• CAS No.: 856061-94-4
• Molecular Formula: C₂₂H₃₀O₂S
• Molecular Weight: 358.545
• Mol file: 856061-94-4.mol

Synonyms:bis-(4-benzyloxy-butyl)-sulfide

Chemical Property of bis-(4-benzyloxy-butyl)-sulfide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of bis-(4-benzyloxy-butyl)-sulfide

There total 10 articles about bis-(4-benzyloxy-butyl)-sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-benzyloxy-butan-1-ol (4541-14-4) → bis-(4-benzyloxy-butyl)-sulfide (856061-94-4)

Guidance literature:

Multi-step reaction with 2 steps

1: dimethylaniline; thionyl chloride

2: aqueous-alcoholic sodium sulfide / Erhitzen des Reaktionsprodukts im Luftstrom unter vermindertem Druck auf 120grad

With sodium sulfide; thionyl chloride; 2,3-Dimethylaniline;

Reference yield:

[(4-chlorobutoxy)methyl]benzene (50873-93-3) → bis-(4-benzyloxy-butyl)-sulfide (856061-94-4)

Guidance literature:

With sodium sulfide; Erhitzen des Reaktionsprodukts im Luftstrom unter vermindertem Druck auf 120grad;

Reference yield:

benzyl 2-chloroethyl ether (17229-17-3) → bis-(4-benzyloxy-butyl)-sulfide (856061-94-4)

Guidance literature:

Multi-step reaction with 6 steps

1: absolute alcohol

2: alcoholic KOH-solution / Ansaeuern mit verd. Schwefelsaeure und Erhitzen des Reaktionsprodukts auf 170-180grad

3: alcoholic sulfuric acid

4: sodium; absolute alcohol; toluene

5: dimethylaniline; thionyl chloride

6: aqueous-alcoholic sodium sulfide / Erhitzen des Reaktionsprodukts im Luftstrom unter vermindertem Druck auf 120grad

With sodium sulfide; potassium hydroxide; thionyl chloride; ethanol; sulfuric acid; sodium; toluene; 2,3-Dimethylaniline;

upstream raw materials:

[(4-chlorobutoxy)methyl]benzene

benzyl 2-chloroethyl ether

3-benzyloxypropan-1-ol

1-chloro-3-benzyloxypropane

Downstream raw materials:

benzyl bromide