N-[(methoxycarbonyl)methyl]-N'-[morpholino(thiocarbonyl)]-3-nitrobenzamidine

Base Information

Chemical Name:N-[(methoxycarbonyl)methyl]-N'-[morpholino(thiocarbonyl)]-3-nitrobenzamidine
CAS No.:189452-68-4
Molecular Formula:C₁₅H₁₈N₄O₅S
Molecular Weight:366.398
Hs Code.:

Synonyms:N-[(methoxycarbonyl)methyl]-N'-[morpholino(thiocarbonyl)]-3-nitrobenzamidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[(methoxycarbonyl)methyl]-N'-[morpholino(thiocarbonyl)]-3-nitrobenzamidine

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Technology Process of N-[(methoxycarbonyl)methyl]-N'-[morpholino(thiocarbonyl)]-3-nitrobenzamidine

There total 2 articles about N-[(methoxycarbonyl)methyl]-N'-[morpholino(thiocarbonyl)]-3-nitrobenzamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 121-90-4
m-nitrobenzoic acid chloride

: 189452-68-4
N-[(methoxycarbonyl)methyl]-N'-[morpholino(thiocarbonyl)]-3-nitrobenzamidine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) MeCN, reflux, 40 min, 2.) MeCN, 30 min

2: 1.) SCCl₂, 2.) Et₃N / 1.) acetone, 15 min, 2.) MeCN, 10 min

With thiophosgene; triethylamine;
DOI:10.1021/jo970072h

Reference yield:

: 5680-79-5,883886-67-7
glycine ethyl ester hydrochloride

: 58415-36-4
N?(3?nitrobenzoyl)morpholine?4?carbothioamide

: 189452-68-4
N-[(methoxycarbonyl)methyl]-N'-[morpholino(thiocarbonyl)]-3-nitrobenzamidine

Guidance literature:: With thiophosgene; triethylamine; Yield given. Multistep reaction; 1.) acetone, 15 min, 2.) MeCN, 10 min;
DOI:10.1021/jo970072h