sodium 2-(benzyloxycarbonylamino)ethyl O-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-(2-acetamido-4,6-di-O-acetyl-2-desoxy-β-D-galactopyranosyl)-(1->4)-(methyl 2,3-di-O-benzoyl-6-O-sulfonato-β-D-glucopyranosyluronate)-(1->3)-2-acetamido-6-O-benzoyl-2-desoxy-β-D-galactopyranoside

Base Information

• Chemical Name: sodium 2-(benzyloxycarbonylamino)ethyl O-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-(2-acetamido-4,6-di-O-acetyl-2-desoxy-β-D-galactopyranosyl)-(1->4)-(methyl 2,3-di-O-benzoyl-6-O-sulfonato-β-D-glucopyranosyluronate)-(1->3)-2-acetamido-6-O-benzoyl-2-desoxy-β-D-galactopyranoside
• CAS No.: 1327313-89-2
• Molecular Formula: C₇₁H₈₀N₃O₃₆S*Na
• Molecular Weight: 1606.47

Synonyms:sodium 2-(benzyloxycarbonylamino)ethyl O-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-(2-acetamido-4,6-di-O-acetyl-2-desoxy-β-D-galactopyranosyl)-(1->4)-(methyl 2,3-di-O-benzoyl-6-O-sulfonato-β-D-glucopyranosyluronate)-(1->3)-2-acetamido-6-O-benzoyl-2-desoxy-β-D-galactopyranoside

Chemical Property of sodium 2-(benzyloxycarbonylamino)ethyl O-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-(2-acetamido-4,6-di-O-acetyl-2-desoxy-β-D-galactopyranosyl)-(1->4)-(methyl 2,3-di-O-benzoyl-6-O-sulfonato-β-D-glucopyranosyluronate)-(1->3)-2-acetamido-6-O-benzoyl-2-desoxy-β-D-galactopyranoside

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Technology Process of sodium 2-(benzyloxycarbonylamino)ethyl O-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-(2-acetamido-4,6-di-O-acetyl-2-desoxy-β-D-galactopyranosyl)-(1->4)-(methyl 2,3-di-O-benzoyl-6-O-sulfonato-β-D-glucopyranosyluronate)-(1->3)-2-acetamido-6-O-benzoyl-2-desoxy-β-D-galactopyranoside

There total 1 articles about sodium 2-(benzyloxycarbonylamino)ethyl O-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-(2-acetamido-4,6-di-O-acetyl-2-desoxy-β-D-galactopyranosyl)-(1->4)-(methyl 2,3-di-O-benzoyl-6-O-sulfonato-β-D-glucopyranosyluronate)-(1->3)-2-acetamido-6-O-benzoyl-2-desoxy-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

2-(benzyloxycarbonylamino)ethyl O-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-(2-acetamido-4,6-di-O-acetyl-2-deoxy-β-D-galactopyranosyl)-(1->4)-(methyl 2,3-di-O-benzoyl-β-D-glucopyranosyluronate)-(1->3)-2-acetamido-4-O-benzoyl-2-deoxy-β-D-galactopyranoside (1327313-83-6) → sodium 2-(benzyloxycarbonylamino)ethyl O-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-(2-acetamido-4,6-di-O-acetyl-2-desoxy-β-D-galactopyranosyl)-(1->4)-(methyl 2,3-di-O-benzoyl-6-O-sulfonato-β-D-glucopyranosyluronate)-(1->3)-2-acetamido-6-O-benzoyl-2-desoxy-β-D-galactopyranoside (1327313-89-2)

Guidance literature:

2-(benzyloxycarbonylamino)ethyl O-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-(2-acetamido-4,6-di-O-acetyl-2-deoxy-β-D-galactopyranosyl)-(1->4)-(methyl 2,3-di-O-benzoyl-β-D-glucopyranosyluronate)-(1->3)-2-acetamido-4-O-benzoyl-2-deoxy-β-D-galactopyranoside; With sulfur trioxide trimethylamine complex; In N,N-dimethyl-formamide; at 60 ℃;

In methanol; dichloromethane; water;

DOI:10.1002/ejoc.201100298

Reference yield: 91.0%

sodium 2-(benzyloxycarbonylamino)ethyl O-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-(2-acetamido-4,6-di-O-acetyl-2-desoxy-β-D-galactopyranosyl)-(1->4)-(methyl 2,3-di-O-benzoyl-6-O-sulfonato-β-D-glucopyranosyluronate)-(1->3)-2-acetamido-6-O-benzoyl-2-desoxy-β-D-galactopyranoside (1327313-89-2) → sodium 2-(benzyloxycarbonylamino)ethyl O-(sodium β-D-glucopyranosyluronate)-(1->3)-(2-acetamido-2-deoxy-β-D-galactopyranosyl)-(1->4)-(sodium β-D-glucopyranosyluronate)-(1->3)-2-acetamido-2-deoxy-6-O-sulfonato-β-D-galactopyranoside

Guidance literature:

sodium 2-(benzyloxycarbonylamino)ethyl O-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-(2-acetamido-4,6-di-O-acetyl-2-desoxy-β-D-galactopyranosyl)-(1->4)-(methyl 2,3-di-O-benzoyl-6-O-sulfonato-β-D-glucopyranosyluronate)-(1->3)-2-acetamido-6-O-benzoyl-2-desoxy-β-D-galactopyranoside; With dihydrogen peroxide; lithium hydroxide; In tetrahydrofuran; water; at -10 - 20 ℃; for 16h;

With sodium hydroxide; In tetrahydrofuran; methanol; water; for 8h;

DOI:10.1002/ejoc.201100298

upstream raw materials:

2-(benzyloxycarbonylamino)ethyl O-(methyl 2,3,4-tri-O-acetyl-β-D-glucopyranosyluronate)-(1->3)-(2-acetamido-4,6-di-O-acetyl-2-deoxy-β-D-galactopyranosyl)-(1->4)-(methyl 2,3-di-O-benzoyl-β-D-glucopyranosyluronate)-(1->3)-2-acetamido-4-O-benzoyl-2-deoxy-β-D-galactopyranoside

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