(2R,3S,5R)-<3-<<(1,1-dimethylethyl)diphenylsilyl>oxy>-5-methyl-2-(1-methylethenyl)-6-oxo-1-piperidinyl>-carbamic acid 2,2,2-trichloroethyl ester

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Chemical Name:(2R,3S,5R)-<3-<<(1,1-dimethylethyl)diphenylsilyl>oxy>-5-methyl-2-(1-methylethenyl)-6-oxo-1-piperidinyl>-carbamic acid 2,2,2-trichloroethyl ester
CAS No.:157465-36-6
Molecular Formula:C₂₈H₃₅Cl₃N₂O₄Si
Molecular Weight:598.041
Hs Code.:

Synonyms:(2R,3S,5R)-<3-<<(1,1-dimethylethyl)diphenylsilyl>oxy>-5-methyl-2-(1-methylethenyl)-6-oxo-1-piperidinyl>-carbamic acid 2,2,2-trichloroethyl ester

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Chemical Property of (2R,3S,5R)-<3-<<(1,1-dimethylethyl)diphenylsilyl>oxy>-5-methyl-2-(1-methylethenyl)-6-oxo-1-piperidinyl>-carbamic acid 2,2,2-trichloroethyl ester

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Technology Process of (2R,3S,5R)-<3-<<(1,1-dimethylethyl)diphenylsilyl>oxy>-5-methyl-2-(1-methylethenyl)-6-oxo-1-piperidinyl>-carbamic acid 2,2,2-trichloroethyl ester

There total 1 articles about (2R,3S,5R)-<3-<<(1,1-dimethylethyl)diphenylsilyl>oxy>-5-methyl-2-(1-methylethenyl)-6-oxo-1-piperidinyl>-carbamic acid 2,2,2-trichloroethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: (4S)-2-<2,6-dimethyl-4-<<(1,1-dimethylethyl)diphenylsilyl>oxy>-1-oxo-5-heptenyl>-hydrazinecarboxylic acid 2,2,2-trichloroethyl ester

: 157465-36-6
(2R,3S,5R)-<3-<<(1,1-dimethylethyl)diphenylsilyl>oxy>-5-methyl-2-(1-methylethenyl)-6-oxo-1-piperidinyl>-carbamic acid 2,2,2-trichloroethyl ester

Guidance literature:: With lead(IV) acetate; In dichloromethane; -20 deg C, 30 min then to 0 deg C, 30 min;
DOI:10.1016/S0040-4020(01)85279-0

Reference yield:

: 157465-36-6
(2R,3S,5R)-<3-<<(1,1-dimethylethyl)diphenylsilyl>oxy>-5-methyl-2-(1-methylethenyl)-6-oxo-1-piperidinyl>-carbamic acid 2,2,2-trichloroethyl ester

: 157465-37-7
(3R,5S,6R)-5-<<(1,1-dimethylethyl)diphenylsilyl>oxy>-3-methyl-6-(1-methylethenyl)-2-piperidinone

Guidance literature:: Multi-step reaction with 2 steps

1: 210 mg / Zn/AcOH / 4 h

2: N-nitrosodiphenylamine / benzene / 4 h / 80 °C / sealed tube

With acetic acid; zinc; N-nitrosodiphenylamine; In benzene;
DOI:10.1016/S0040-4020(01)85279-0