N-(2-(triphenylsilyl)ethoxy)carbonyl-L-leucine allyl ester

Base Information

Chemical Name:N-(2-(triphenylsilyl)ethoxy)carbonyl-L-leucine allyl ester
CAS No.:1310360-92-9
Molecular Formula:C₃₀H₃₅NO₄Si
Molecular Weight:501.698
Hs Code.:

Synonyms:N-(2-(triphenylsilyl)ethoxy)carbonyl-L-leucine allyl ester

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Chemical Property of N-(2-(triphenylsilyl)ethoxy)carbonyl-L-leucine allyl ester

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Technology Process of N-(2-(triphenylsilyl)ethoxy)carbonyl-L-leucine allyl ester

There total 3 articles about N-(2-(triphenylsilyl)ethoxy)carbonyl-L-leucine allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1310360-86-1
4-nitrophenyl 2-(triphenylsilyl)ethyl carbonate

: 88224-03-7
L-leucine allyl ester hydro-p-toluenesulfonate

: 1310360-92-9
N-(2-(triphenylsilyl)ethoxy)carbonyl-L-leucine allyl ester

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.3390/molecules16064695

Reference yield:

: 18666-68-7
vinyltriphenylsilane

: 1310360-92-9
N-(2-(triphenylsilyl)ethoxy)carbonyl-L-leucine allyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 3 h / Inert atmosphere; Reflux

1.2: 3 h / 45 °C / Inert atmosphere

2.1: pyridine / dichloromethane / 24 h / 20 °C / Inert atmosphere

3.1: triethylamine / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

With pyridine; triethylamine; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.3390/molecules16064695

Reference yield:

: 18666-87-0
1,1,1-triphenyl-1-silapropan-3-ol

: 1310360-92-9
N-(2-(triphenylsilyl)ethoxy)carbonyl-L-leucine allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / dichloromethane / 24 h / 20 °C / Inert atmosphere

2: triethylamine / N,N-dimethyl-formamide / 24 h / 20 °C / Inert atmosphere

With pyridine; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.3390/molecules16064695