3,5-di-t-butyl-4-hydroxy-N,N-dimethyl-N-<(2E)-2-methylpenta-2,4-dienyl>anilinium bromide

Base Information

Chemical Name:3,5-di-t-butyl-4-hydroxy-N,N-dimethyl-N-<(2E)-2-methylpenta-2,4-dienyl>anilinium bromide
CAS No.:50998-91-9
Molecular Formula:Br*C₂₂H₃₆NO
Molecular Weight:410.438
Hs Code.:

Synonyms:3,5-di-t-butyl-4-hydroxy-N,N-dimethyl-N-<(2E)-2-methylpenta-2,4-dienyl>anilinium bromide

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Chemical Property of 3,5-di-t-butyl-4-hydroxy-N,N-dimethyl-N-<(2E)-2-methylpenta-2,4-dienyl>anilinium bromide

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Technology Process of 3,5-di-t-butyl-4-hydroxy-N,N-dimethyl-N-<(2E)-2-methylpenta-2,4-dienyl>anilinium bromide

There total 1 articles about 3,5-di-t-butyl-4-hydroxy-N,N-dimethyl-N-<(2E)-2-methylpenta-2,4-dienyl>anilinium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 10437-44-2
N,N-dimethyl-2,6-ditertiarybutyl-4-amino phenol

: 50999-02-5
(2E)-2-methylpenta-2,4-dienyl bromide

: 50998-91-9
3,5-di-t-butyl-4-hydroxy-N,N-dimethyl-N-<(2E)-2-methylpenta-2,4-dienyl>anilinium bromide

Guidance literature:: In acetonitrile;

Reference yield: 88.0%

: 50998-91-9
3,5-di-t-butyl-4-hydroxy-N,N-dimethyl-N-<(2E)-2-methylpenta-2,4-dienyl>anilinium bromide

: 50998-95-3
2,6-di-t-butyl-4-dimethylamino-2<(2E)-4-methylpenta-2,4-dienyl>cyclohexa-3,5-dienone

Guidance literature:: With sodium methylate; In methanol; at 0 ℃; for 4h;

Reference yield:

: 50998-91-9
3,5-di-t-butyl-4-hydroxy-N,N-dimethyl-N-<(2E)-2-methylpenta-2,4-dienyl>anilinium bromide

: 51094-12-3
2,6-di-t-butyl-2<(2E)-4-methylpenta-2,4-dienyl>cyclohex-5-ene-1,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / sodium methoxide / methanol / 4 h / 0 °C

2: 20 percent / H₂O/SiO₂ / 12 h

With water; sodium methylate; silica gel; In methanol;