C₈H₉BrN₂OS

Base Information

• Chemical Name: C₈H₉BrN₂OS
• CAS No.: 1260248-72-3
• Molecular Formula: C₈H₉BrN₂OS
• Molecular Weight: 261.142
• Mol file: 1260248-72-3.mol

Synonyms:C₈H₉BrN₂OS

Chemical Property of C₈H₉BrN₂OS

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₈H₉BrN₂OS

There total 2 articles about C₈H₉BrN₂OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-bromo-1-isothiocyanato-4-methoxy-benzene → C8H9BrN2OS (1260248-72-3)

Guidance literature:

With ammonium hydroxide; In water; ethyl acetate; at 20 ℃;

DOI:10.1080/00397911.2010.532276

Reference yield:

C6H15N*C8H8BrNOS2 (1189351-09-4) → C8H9BrN2OS (1260248-72-3)

Guidance literature:

Multi-step reaction with 2 steps

1: iodine; sodium hydrogencarbonate / water; ethyl acetate

2: ammonium hydroxide / water; ethyl acetate / 20 °C

With ammonium hydroxide; iodine; sodium hydrogencarbonate; In water; ethyl acetate;

DOI:10.1080/00397911.2010.532276

Reference yield: 91.0%

C8H9BrN2OS (1260248-72-3) → (2-bromo-4-methoxyphenyl)cyanamide (1260248-88-1)

Guidance literature:

With copper(l) iodide; sodium hydroxide; In dimethyl sulfoxide; at 90 ℃; for 1.5h;

DOI:10.1002/adsc.201000383

upstream raw materials:

C₆H₁₅N*C₈H₈BrNOS₂

Downstream raw materials:

(2-bromo-4-methoxyphenyl)cyanamide

4-methoxy-2-(phenylthio)phenylcyanamide

6-methoxy-N-(2-nitrophenyl)benzo[d]thiazol-2-amine

2-(2-nitrophenylthio)-4-methoxyphenylcyanamide