dimethyl 5-(6-(4-cyano-2-fluorobenzyloxy)naphthalene-2-sulfonamido)isophthalate

Base Information

Chemical Name:dimethyl 5-(6-(4-cyano-2-fluorobenzyloxy)naphthalene-2-sulfonamido)isophthalate
CAS No.:1312919-76-8
Molecular Formula:C₂₈H₂₁FN₂O₇S
Molecular Weight:548.548
Hs Code.:

Synonyms:dimethyl 5-(6-(4-cyano-2-fluorobenzyloxy)naphthalene-2-sulfonamido)isophthalate

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Chemical Property of dimethyl 5-(6-(4-cyano-2-fluorobenzyloxy)naphthalene-2-sulfonamido)isophthalate

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Technology Process of dimethyl 5-(6-(4-cyano-2-fluorobenzyloxy)naphthalene-2-sulfonamido)isophthalate

There total 3 articles about dimethyl 5-(6-(4-cyano-2-fluorobenzyloxy)naphthalene-2-sulfonamido)isophthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1092117-57-1
C₁₈H₁₁ClFNO₃S

: 99-27-4
dimethyl 5-aminoisophthalate

: 1312919-76-8
dimethyl 5-(6-(4-cyano-2-fluorobenzyloxy)naphthalene-2-sulfonamido)isophthalate

Guidance literature:: With triethylamine; In ethanol; at 55 ℃; for 48h; Inert atmosphere;
DOI:10.1016/j.ejmech.2011.04.011

Reference yield:

: 135-76-2
sodium 2-naphthol-6-sulfonate

: 1312919-76-8
dimethyl 5-(6-(4-cyano-2-fluorobenzyloxy)naphthalene-2-sulfonamido)isophthalate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium / ethanol / 20 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

1.3: 0 - 20 °C / Inert atmosphere

2.1: triethylamine / ethanol / 48 h / 55 °C / Inert atmosphere

With sodium; triethylamine; In ethanol;
DOI:10.1016/j.ejmech.2011.04.011

Reference yield:

: 105942-09-4
4-(bromomethyl)-3-fluorobenzonitrile

: 1312919-76-8
dimethyl 5-(6-(4-cyano-2-fluorobenzyloxy)naphthalene-2-sulfonamido)isophthalate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium / ethanol / 20 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

1.3: 0 - 20 °C / Inert atmosphere

2.1: triethylamine / ethanol / 48 h / 55 °C / Inert atmosphere

With sodium; triethylamine; In ethanol;
DOI:10.1016/j.ejmech.2011.04.011