Technology Process of C24H31N7O5
There total 10 articles about C24H31N7O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl acetamide / 0.08 h
1.2: 100 °C
1.3: 3 h / 20 - 30 °C
2.1: magnesium sulfate / N,N-dimethyl acetamide / 80 °C
3.1: trifluoroacetic acid / 6 h / 20 °C
With
magnesium sulfate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid;
In
N,N-dimethyl acetamide;
- Guidance literature:
-
With
trifluoroacetic acid;
at 20 ℃;
for 6h;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: caesium carbonate / toluene / 0.33 h / 40 °C
1.2: Heating / reflux
2.1: hydrogenchloride / 1,4-dioxane / 30 h / 100 °C
3.1: caesium carbonate / N,N-dimethyl acetamide / 60 °C
4.1: thiophene; hydrogen / palladium 10% on activated carbon / ethanol; di-isopropyl ether / 20 h / 20 °C
4.2: 0 °C
5.1: hydrogenchloride; water / 1,4-dioxane / 10 h / 50 °C
6.1: magnesium sulfate / N,N-dimethyl acetamide / 80 °C
7.1: trifluoroacetic acid / 6 h / 20 °C
With
thiophene; hydrogenchloride; water; hydrogen; magnesium sulfate; caesium carbonate; trifluoroacetic acid;
palladium 10% on activated carbon;
In
1,4-dioxane; ethanol; di-isopropyl ether; N,N-dimethyl acetamide; toluene;