C₂₃H₂₈O₄

Base Information

Chemical Name:C₂₃H₂₈O₄
CAS No.:954416-37-6
Molecular Formula:C₂₃H₂₈O₄
Molecular Weight:368.473
Hs Code.:

C<sub>23</sub>H<sub>28</sub>O<sub>4</sub>

Synonyms:C₂₃H₂₈O₄

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Chemical Property of C₂₃H₂₈O₄

Chemical Property:

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Technology Process of C₂₃H₂₈O₄

There total 9 articles about C₂₃H₂₈O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 954416-32-1
C₂₁H₂₈O₃Si

: 954416-37-6
C₂₃H₂₈O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: 80 percent / NaH; TBAI / tetrahydrofuran / 12 h / 0 °C

2.1: NMO; OsO₄ / acetone; H₂O / 24 h / 20 °C

2.2: NaIO₄ / tetrahydrofuran; H₂O / 1 h / 0 °C

2.3: 70 percent / CH₂Cl₂ / 6 h / 20 °C

3.1: 90 percent / H₂; n-BuNH₂ / Pd/C / methanol / 2 h / 20 °C

4.1: 90 percent / TBAF / tetrahydrofuran / 6 h / 20 °C

5.1: (COCl)2; Et₃N; DMSO / CH₂Cl₂ / 0.5 h / -78 °C

5.2: 75 percent / diethyl ether / 0 °C

With osmium(VIII) oxide; N-methyl-2-indolinone; oxalyl dichloride; tetrabutyl ammonium fluoride; hydrogen; tetra-(n-butyl)ammonium iodide; sodium hydride; dimethyl sulfoxide; N-butylamine; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; acetone; 2.3: Wittig olefination reaction / 5.1: Swern oxidation reaction / 5.2: Wittig olefination reaction;
DOI:10.1016/j.tetlet.2007.07.176

Reference yield:

: 954416-34-3
C₃₈H₄₄O₅Si

: 954416-37-6
C₂₃H₂₈O₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: 90 percent / H₂; n-BuNH₂ / Pd/C / methanol / 2 h / 20 °C

2.1: 90 percent / TBAF / tetrahydrofuran / 6 h / 20 °C

3.1: (COCl)2; Et₃N; DMSO / CH₂Cl₂ / 0.5 h / -78 °C

3.2: 75 percent / diethyl ether / 0 °C

With oxalyl dichloride; tetrabutyl ammonium fluoride; hydrogen; dimethyl sulfoxide; N-butylamine; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; 3.1: Swern oxidation reaction / 3.2: Wittig olefination reaction;
DOI:10.1016/j.tetlet.2007.07.176

Reference yield:

: 954416-33-2
C₃₅H₄₀O₃Si

: 954416-37-6
C₂₃H₂₈O₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: NMO; OsO₄ / acetone; H₂O / 24 h / 20 °C

1.2: NaIO₄ / tetrahydrofuran; H₂O / 1 h / 0 °C

1.3: 70 percent / CH₂Cl₂ / 6 h / 20 °C

2.1: 90 percent / H₂; n-BuNH₂ / Pd/C / methanol / 2 h / 20 °C

3.1: 90 percent / TBAF / tetrahydrofuran / 6 h / 20 °C

4.1: (COCl)2; Et₃N; DMSO / CH₂Cl₂ / 0.5 h / -78 °C

4.2: 75 percent / diethyl ether / 0 °C

With osmium(VIII) oxide; N-methyl-2-indolinone; oxalyl dichloride; tetrabutyl ammonium fluoride; hydrogen; dimethyl sulfoxide; N-butylamine; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; acetone; 1.3: Wittig olefination reaction / 4.1: Swern oxidation reaction / 4.2: Wittig olefination reaction;
DOI:10.1016/j.tetlet.2007.07.176