2-<3-phenylacetamido-4-benzylthiocarbonate-(3R,4R)-azetidin-2-on-1-yl>-allyl acetate

Base Information

Chemical Name:2-<3-phenylacetamido-4-benzylthiocarbonate-(3R,4R)-azetidin-2-on-1-yl>-allyl acetate
CAS No.:122691-89-8
Molecular Formula:C₂₄H₂₄N₂O₆S
Molecular Weight:468.53
Hs Code.:

Synonyms:2-<3-phenylacetamido-4-benzylthiocarbonate-(3R,4R)-azetidin-2-on-1-yl>-allyl acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-<3-phenylacetamido-4-benzylthiocarbonate-(3R,4R)-azetidin-2-on-1-yl>-allyl acetate

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Technology Process of 2-<3-phenylacetamido-4-benzylthiocarbonate-(3R,4R)-azetidin-2-on-1-yl>-allyl acetate

There total 2 articles about 2-<3-phenylacetamido-4-benzylthiocarbonate-(3R,4R)-azetidin-2-on-1-yl>-allyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 501-53-1,94274-21-2
benzyl chloroformate

: 124166-16-1
2-<3-phenylacetamido-4-thiol-(3R,4R)-azetidin-2-on-1-yl>-allyl acetate

: 122691-89-8
2-<3-phenylacetamido-4-benzylthiocarbonate-(3R,4R)-azetidin-2-on-1-yl>-allyl acetate

Guidance literature:: With triethylamine; In dichloromethane; for 2h; Ambient temperature;
DOI:10.1016/0223-5234(88)90100-6

Reference yield:

: 87996-79-0
2-<3-benzyl-6-oxo-2-thia-4,7-diaza-(1R,5R)-bicyclo-<3.2.0>-hept-3-en-7-yl>-allyl acetate

: 122691-89-8
2-<3-phenylacetamido-4-benzylthiocarbonate-(3R,4R)-azetidin-2-on-1-yl>-allyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / 1.2 N aq HCl / dimethylformamide / 1 h / Ambient temperature

2: 79 percent / triethylamine / CH₂Cl₂ / 2 h / Ambient temperature

With hydrogenchloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/0223-5234(88)90100-6