allyl 2-acetylamino-2-deoxy-3,4-dibenzyl-6-O-(3,4-O-dibenzyl-α-L-rhamnopyranosyl)-α-D-glucopyranoside

Base Information

Chemical Name:allyl 2-acetylamino-2-deoxy-3,4-dibenzyl-6-O-(3,4-O-dibenzyl-α-L-rhamnopyranosyl)-α-D-glucopyranoside
CAS No.:167013-80-1
Molecular Formula:C₄₅H₅₃NO₁₀
Molecular Weight:767.917
Hs Code.:

Synonyms:allyl 2-acetylamino-2-deoxy-3,4-dibenzyl-6-O-(3,4-O-dibenzyl-α-L-rhamnopyranosyl)-α-D-glucopyranoside

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Chemical Property of allyl 2-acetylamino-2-deoxy-3,4-dibenzyl-6-O-(3,4-O-dibenzyl-α-L-rhamnopyranosyl)-α-D-glucopyranoside

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Technology Process of allyl 2-acetylamino-2-deoxy-3,4-dibenzyl-6-O-(3,4-O-dibenzyl-α-L-rhamnopyranosyl)-α-D-glucopyranoside

There total 4 articles about allyl 2-acetylamino-2-deoxy-3,4-dibenzyl-6-O-(3,4-O-dibenzyl-α-L-rhamnopyranosyl)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.7%

: 167013-79-8
allyl 2-acetylamino-2-deoxy-3,4-dibenzyl-6-O-(2-O-acetyl-3,4-O-dibenzyl-α-L-rhamnopyranosyl)-α-D-glucopyranoside

: 167013-80-1
allyl 2-acetylamino-2-deoxy-3,4-dibenzyl-6-O-(3,4-O-dibenzyl-α-L-rhamnopyranosyl)-α-D-glucopyranoside

Guidance literature:: With potassium carbonate; In methanol; for 1h; Ambient temperature;
DOI:10.1016/S0957-4166(00)86306-5

Reference yield:

: 63064-56-2
allyl 2-acetylamino-2-deoxy-3,4-O-dibenzyl-6-O-trityl-α-D-glucopyranoside

: 167013-80-1
allyl 2-acetylamino-2-deoxy-3,4-dibenzyl-6-O-(3,4-O-dibenzyl-α-L-rhamnopyranosyl)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 74.2 percent / NaI, Me₃SiCl / acetonitrile / 0.25 h

2: 1.) NaH, 4AMS, 2.) BF₃*Et₂O, 4AMS / 1.) CCl₃CN, CH₂Cl₂, RT, 40 min, 2.) CCl₃CN, CH₂Cl₂, 2 h

3: 94.7 percent / K₂CO₃ / methanol / 1 h / Ambient temperature

With chloro-trimethyl-silane; boron trifluoride diethyl etherate; sodium hydride; potassium carbonate; sodium iodide; In methanol; acetonitrile;
DOI:10.1016/S0957-4166(00)86306-5

Reference yield:

: 73983-18-3
2-O-acetyl-3,4-O-dibenzyl-α-L-rhamnopyranoside

: 167013-80-1
allyl 2-acetylamino-2-deoxy-3,4-dibenzyl-6-O-(3,4-O-dibenzyl-α-L-rhamnopyranosyl)-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH, 4AMS, 2.) BF₃*Et₂O, 4AMS / 1.) CCl₃CN, CH₂Cl₂, RT, 40 min, 2.) CCl₃CN, CH₂Cl₂, 2 h

2: 94.7 percent / K₂CO₃ / methanol / 1 h / Ambient temperature

With boron trifluoride diethyl etherate; sodium hydride; potassium carbonate; In methanol;
DOI:10.1016/S0957-4166(00)86306-5