6-methyl-N₁-(4-(5-(pyrrolidin-1-yl)pyridin-3-yl)pyrimidin-2-yl)benzene-1,3-diamine

Base Information

• Chemical Name: 6-methyl-N₁-(4-(5-(pyrrolidin-1-yl)pyridin-3-yl)pyrimidin-2-yl)benzene-1,3-diamine
• CAS No.: 1079880-79-7
• Molecular Formula: C₂₀H₂₂N₆
• Molecular Weight: 346.435

Synonyms:6-methyl-N₁-(4-(5-(pyrrolidin-1-yl)pyridin-3-yl)pyrimidin-2-yl)benzene-1,3-diamine

Chemical Property of 6-methyl-N₁-(4-(5-(pyrrolidin-1-yl)pyridin-3-yl)pyrimidin-2-yl)benzene-1,3-diamine

Chemical Property:

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Technology Process of 6-methyl-N₁-(4-(5-(pyrrolidin-1-yl)pyridin-3-yl)pyrimidin-2-yl)benzene-1,3-diamine

There total 2 articles about 6-methyl-N₁-(4-(5-(pyrrolidin-1-yl)pyridin-3-yl)pyrimidin-2-yl)benzene-1,3-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C20H20N6O2 (1079880-77-5) → 6-methyl-N1-(4-(5-(pyrrolidin-1-yl)pyridin-3-yl)pyrimidin-2-yl)benzene-1,3-diamine (1079880-79-7)

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In ethanol; at 20 ℃; under 760.051 Torr;

Reference yield:

4-(5-bromopyridin-3-yl)-N-(2-methyl-5-nitrophenyl)pyrimidin-2-amine (641615-41-0) → 6-methyl-N1-(4-(5-(pyrrolidin-1-yl)pyridin-3-yl)pyrimidin-2-yl)benzene-1,3-diamine (1079880-79-7)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium phosphate; copper(l) iodide; L-proline / dimethyl sulfoxide / 0.33 h / 160 °C / Microwave irradiation

2: hydrogen / palladium 10% on activated carbon / ethanol / 20 °C / 760.05 Torr

With potassium phosphate; copper(l) iodide; hydrogen; L-proline; palladium 10% on activated carbon; In ethanol; dimethyl sulfoxide;

upstream raw materials:

C₂₀H₂₀N₆O₂

4-(5-bromopyridin-3-yl)-N-(2-methyl-5-nitrophenyl)pyrimidin-2-amine

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