S-[3-cyano-2-oxo-3-(triphenyl-λ5-phosphanylidene)propyl]-O-ethyl carbonodithioate

Base Information

Chemical Name:S-[3-cyano-2-oxo-3-(triphenyl-λ5-phosphanylidene)propyl]-O-ethyl carbonodithioate
CAS No.:1560960-62-4
Molecular Formula:C₂₅H₂₂NO₂PS₂
Molecular Weight:463.561
Hs Code.:

Synonyms:S-[3-cyano-2-oxo-3-(triphenyl-λ5-phosphanylidene)propyl]-O-ethyl carbonodithioate

Suppliers and Price of S-[3-cyano-2-oxo-3-(triphenyl-λ5-phosphanylidene)propyl]-O-ethyl carbonodithioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of S-[3-cyano-2-oxo-3-(triphenyl-λ5-phosphanylidene)propyl]-O-ethyl carbonodithioate

Chemical Property:

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Technology Process of S-[3-cyano-2-oxo-3-(triphenyl-λ5-phosphanylidene)propyl]-O-ethyl carbonodithioate

There total 2 articles about S-[3-cyano-2-oxo-3-(triphenyl-λ5-phosphanylidene)propyl]-O-ethyl carbonodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 20341-88-2
4-chloro-3-oxo-2-(triphenyl-λ5-phosphanylidene)butanenitrile

: 140-89-6
potassium ethyl xanthogenate

: 1560960-62-4
S-[3-cyano-2-oxo-3-(triphenyl-λ5-phosphanylidene)propyl]-O-ethyl carbonodithioate

Guidance literature:: In acetone; at 0 - 20 ℃; for 2.5h; Inert atmosphere;

Reference yield:

: 16640-68-9
cyanomethylene triphenylphosphorane

: 1560960-62-4
S-[3-cyano-2-oxo-3-(triphenyl-λ5-phosphanylidene)propyl]-O-ethyl carbonodithioate

Guidance literature:: Multi-step reaction with 2 steps

1: bovine serum albumin / dichloromethane

2: acetone / 2.5 h / 0 - 20 °C

With bovine serum albumin; In dichloromethane; acetone;
DOI:10.5012/bkcs.2013.34.12.3545

Reference yield: 78.0%

: 94-66-6
2-allylcyclohexan-1-one

: 1560960-62-4
S-[3-cyano-2-oxo-3-(triphenyl-λ5-phosphanylidene)propyl]-O-ethyl carbonodithioate

: S-[6-cyano-5-oxo-1-(2-oxocyclohexyl)-6-(triphenyl-λ5-phosphanylidene)hexan-2-yl] O-ethyl carbonodithioate

: 3-oxo-7-(2-oxocyclohexyl)-2-(triphenyl-λ5-phosphanylidene)heptaneniltrile

Guidance literature:: 2-allylcyclohexan-1-one; S-[3-cyano-2-oxo-3-(triphenyl-λ5-phosphanylidene)propyl]-O-ethyl carbonodithioate; In 1,2-dichloro-ethane; for 0.25h; Reflux; Inert atmosphere;

With dilauryl peroxide; In 1,2-dichloro-ethane; for 3h; Reflux; Inert atmosphere;